[{"user_id":"23547","_id":"25991","page":"4151-4156","status":"public","quality_controlled":"1","citation":{"ieee":"J. Roggenbuck, G. Koch, and M. Tiemann, “Synthesis of Mesoporous Magnesium Oxide by CMK-3 Carbon Structure Replication,” <i>Chemistry of Materials</i>, pp. 4151–4156, 2006, doi: <a href=\"https://doi.org/10.1021/cm060740s\">10.1021/cm060740s</a>.","apa":"Roggenbuck, J., Koch, G., &#38; Tiemann, M. (2006). Synthesis of Mesoporous Magnesium Oxide by CMK-3 Carbon Structure Replication. <i>Chemistry of Materials</i>, 4151–4156. <a href=\"https://doi.org/10.1021/cm060740s\">https://doi.org/10.1021/cm060740s</a>","chicago":"Roggenbuck, Jan, Günter Koch, and Michael Tiemann. “Synthesis of Mesoporous Magnesium Oxide by CMK-3 Carbon Structure Replication.” <i>Chemistry of Materials</i>, 2006, 4151–56. <a href=\"https://doi.org/10.1021/cm060740s\">https://doi.org/10.1021/cm060740s</a>.","short":"J. Roggenbuck, G. Koch, M. Tiemann, Chemistry of Materials (2006) 4151–4156.","mla":"Roggenbuck, Jan, et al. “Synthesis of Mesoporous Magnesium Oxide by CMK-3 Carbon Structure Replication.” <i>Chemistry of Materials</i>, 2006, pp. 4151–56, doi:<a href=\"https://doi.org/10.1021/cm060740s\">10.1021/cm060740s</a>.","bibtex":"@article{Roggenbuck_Koch_Tiemann_2006, title={Synthesis of Mesoporous Magnesium Oxide by CMK-3 Carbon Structure Replication}, DOI={<a href=\"https://doi.org/10.1021/cm060740s\">10.1021/cm060740s</a>}, journal={Chemistry of Materials}, author={Roggenbuck, Jan and Koch, Günter and Tiemann, Michael}, year={2006}, pages={4151–4156} }","ama":"Roggenbuck J, Koch G, Tiemann M. Synthesis of Mesoporous Magnesium Oxide by CMK-3 Carbon Structure Replication. <i>Chemistry of Materials</i>. Published online 2006:4151-4156. doi:<a href=\"https://doi.org/10.1021/cm060740s\">10.1021/cm060740s</a>"},"doi":"10.1021/cm060740s","language":[{"iso":"eng"}],"article_type":"original","date_updated":"2023-03-09T08:58:00Z","publication_status":"published","publication_identifier":{"issn":["0897-4756","1520-5002"]},"author":[{"last_name":"Roggenbuck","first_name":"Jan","full_name":"Roggenbuck, Jan"},{"first_name":"Günter","last_name":"Koch","full_name":"Koch, Günter"},{"full_name":"Tiemann, Michael","orcid":"0000-0003-1711-2722","first_name":"Michael","last_name":"Tiemann","id":"23547"}],"year":"2006","title":"Synthesis of Mesoporous Magnesium Oxide by CMK-3 Carbon Structure Replication","department":[{"_id":"35"},{"_id":"2"},{"_id":"307"}],"type":"journal_article","date_created":"2021-10-09T09:45:04Z","abstract":[{"text":"Periodically ordered mesoporous magnesium oxide was synthesized in a double replication procedure. Mesoporous SBA-15 silica and CMK-3 carbon were successively used as hard structure matrixes. The carbon pore system was infiltrated with Mg(NO3)2, which was then converted to MgO at 573 K; the carbon matrix was finally removed by thermal combustion. The structure of the mesoporous MgO corresponds to that of the original SBA-15 silica. The products consist of hexagonally arranged cylindrical mesopores and crystalline pore walls. The efficiency of the replication series was studied by variation of the infiltration method and comprehensive pore size analysis of all involved mesoporous materials. The in situ formation of MgO inside the CMK-3 carbon pore system was monitored by thermal analysis. Postsynthetic treatment of the products at 823 K in a vacuum prior to removal of the carbon matrix was found to improve the crystallinity but to diminish the periodic order of the pore system.","lang":"eng"}],"extern":"1","publication":"Chemistry of Materials"},{"citation":{"ieee":"M. Tiemann, Ö. Weiß, J. Hartikainen, F. Marlow, and M. Lindén, “Early Stages of ZnS Nanoparticle Growth Studied by In-Situ Stopped-Flow UV Absorption Spectroscopy,” <i>ChemPhysChem</i>, pp. 2113–2119, 2005, doi: <a href=\"https://doi.org/10.1002/cphc.200500163\">10.1002/cphc.200500163</a>.","mla":"Tiemann, Michael, et al. “Early Stages of ZnS Nanoparticle Growth Studied by In-Situ Stopped-Flow UV Absorption Spectroscopy.” <i>ChemPhysChem</i>, 2005, pp. 2113–19, doi:<a href=\"https://doi.org/10.1002/cphc.200500163\">10.1002/cphc.200500163</a>.","apa":"Tiemann, M., Weiß, Ö., Hartikainen, J., Marlow, F., &#38; Lindén, M. (2005). Early Stages of ZnS Nanoparticle Growth Studied by In-Situ Stopped-Flow UV Absorption Spectroscopy. <i>ChemPhysChem</i>, 2113–2119. <a href=\"https://doi.org/10.1002/cphc.200500163\">https://doi.org/10.1002/cphc.200500163</a>","bibtex":"@article{Tiemann_Weiß_Hartikainen_Marlow_Lindén_2005, title={Early Stages of ZnS Nanoparticle Growth Studied by In-Situ Stopped-Flow UV Absorption Spectroscopy}, DOI={<a href=\"https://doi.org/10.1002/cphc.200500163\">10.1002/cphc.200500163</a>}, journal={ChemPhysChem}, author={Tiemann, Michael and Weiß, Özlem and Hartikainen, Juha and Marlow, Frank and Lindén, Mika}, year={2005}, pages={2113–2119} }","short":"M. Tiemann, Ö. Weiß, J. Hartikainen, F. Marlow, M. Lindén, ChemPhysChem (2005) 2113–2119.","ama":"Tiemann M, Weiß Ö, Hartikainen J, Marlow F, Lindén M. Early Stages of ZnS Nanoparticle Growth Studied by In-Situ Stopped-Flow UV Absorption Spectroscopy. <i>ChemPhysChem</i>. Published online 2005:2113-2119. doi:<a href=\"https://doi.org/10.1002/cphc.200500163\">10.1002/cphc.200500163</a>","chicago":"Tiemann, Michael, Özlem Weiß, Juha Hartikainen, Frank Marlow, and Mika Lindén. “Early Stages of ZnS Nanoparticle Growth Studied by In-Situ Stopped-Flow UV Absorption Spectroscopy.” <i>ChemPhysChem</i>, 2005, 2113–19. <a href=\"https://doi.org/10.1002/cphc.200500163\">https://doi.org/10.1002/cphc.200500163</a>."},"quality_controlled":"1","_id":"25995","page":"2113-2119","user_id":"23547","status":"public","date_created":"2021-10-09T09:48:34Z","department":[{"_id":"35"},{"_id":"2"},{"_id":"307"}],"type":"journal_article","publication":"ChemPhysChem","extern":"1","abstract":[{"text":"The early stages of ZnS nanoparticle growth from supersaturated solution are investigated in situ by stopped-flow UV absorption spectroscopy with a time resolution of 1.28 ms. A model for data analysis is suggested which makes it possible to study both the average particle radius and the concentration. The average radii lie in the sub-nanometer range. During the first 40 ms, growth is predominantly governed by ripening.","lang":"eng"}],"language":[{"iso":"eng"}],"doi":"10.1002/cphc.200500163","author":[{"id":"23547","first_name":"Michael","last_name":"Tiemann","orcid":"0000-0003-1711-2722","full_name":"Tiemann, Michael"},{"last_name":"Weiß","first_name":"Özlem","full_name":"Weiß, Özlem"},{"first_name":"Juha","last_name":"Hartikainen","full_name":"Hartikainen, Juha"},{"first_name":"Frank","last_name":"Marlow","full_name":"Marlow, Frank"},{"first_name":"Mika","last_name":"Lindén","full_name":"Lindén, Mika"}],"publication_identifier":{"issn":["1439-4235","1439-7641"]},"title":"Early Stages of ZnS Nanoparticle Growth Studied by In-Situ Stopped-Flow UV Absorption Spectroscopy","year":"2005","article_type":"original","publication_status":"published","date_updated":"2023-03-09T08:58:26Z"},{"publication_identifier":{"issn":["0002-7863","1520-5126"]},"author":[{"first_name":"Jan","last_name":"Roggenbuck","full_name":"Roggenbuck, Jan"},{"orcid":"0000-0003-1711-2722","last_name":"Tiemann","first_name":"Michael","full_name":"Tiemann, Michael","id":"23547"}],"year":"2005","title":"Ordered Mesoporous Magnesium Oxide with High Thermal Stability Synthesized by Exotemplating Using CMK-3 Carbon","article_type":"original","date_updated":"2023-03-09T08:58:46Z","publication_status":"published","language":[{"iso":"eng"}],"doi":"10.1021/ja043605u","publication":"Journal of the American Chemical Society","abstract":[{"lang":"eng","text":"Periodically ordered mesoporous magnesium oxides were synthesized by utilization of mesoporous CMK-3 carbon as exotemplate. The products exhibit high thermal stability and basic properties, which makes them promising for application in heterogeneous basic catalysis."}],"extern":"1","date_created":"2021-10-09T09:47:51Z","department":[{"_id":"35"},{"_id":"2"},{"_id":"307"}],"type":"journal_article","status":"public","_id":"25994","page":"1096-1097","user_id":"23547","citation":{"bibtex":"@article{Roggenbuck_Tiemann_2005, title={Ordered Mesoporous Magnesium Oxide with High Thermal Stability Synthesized by Exotemplating Using CMK-3 Carbon}, DOI={<a href=\"https://doi.org/10.1021/ja043605u\">10.1021/ja043605u</a>}, journal={Journal of the American Chemical Society}, author={Roggenbuck, Jan and Tiemann, Michael}, year={2005}, pages={1096–1097} }","short":"J. Roggenbuck, M. Tiemann, Journal of the American Chemical Society (2005) 1096–1097.","ama":"Roggenbuck J, Tiemann M. Ordered Mesoporous Magnesium Oxide with High Thermal Stability Synthesized by Exotemplating Using CMK-3 Carbon. <i>Journal of the American Chemical Society</i>. Published online 2005:1096-1097. doi:<a href=\"https://doi.org/10.1021/ja043605u\">10.1021/ja043605u</a>","chicago":"Roggenbuck, Jan, and Michael Tiemann. “Ordered Mesoporous Magnesium Oxide with High Thermal Stability Synthesized by Exotemplating Using CMK-3 Carbon.” <i>Journal of the American Chemical Society</i>, 2005, 1096–97. <a href=\"https://doi.org/10.1021/ja043605u\">https://doi.org/10.1021/ja043605u</a>.","ieee":"J. Roggenbuck and M. Tiemann, “Ordered Mesoporous Magnesium Oxide with High Thermal Stability Synthesized by Exotemplating Using CMK-3 Carbon,” <i>Journal of the American Chemical Society</i>, pp. 1096–1097, 2005, doi: <a href=\"https://doi.org/10.1021/ja043605u\">10.1021/ja043605u</a>.","apa":"Roggenbuck, J., &#38; Tiemann, M. (2005). Ordered Mesoporous Magnesium Oxide with High Thermal Stability Synthesized by Exotemplating Using CMK-3 Carbon. <i>Journal of the American Chemical Society</i>, 1096–1097. <a href=\"https://doi.org/10.1021/ja043605u\">https://doi.org/10.1021/ja043605u</a>","mla":"Roggenbuck, Jan, and Michael Tiemann. “Ordered Mesoporous Magnesium Oxide with High Thermal Stability Synthesized by Exotemplating Using CMK-3 Carbon.” <i>Journal of the American Chemical Society</i>, 2005, pp. 1096–97, doi:<a href=\"https://doi.org/10.1021/ja043605u\">10.1021/ja043605u</a>."},"quality_controlled":"1"},{"department":[{"_id":"35"},{"_id":"2"},{"_id":"307"}],"type":"journal_article","date_created":"2021-10-09T09:49:26Z","extern":"1","abstract":[{"lang":"eng","text":"In situ Synchrotron SAXS/XRD Study on the Formation of Ordered Mesoscopic Hybrid Materials with Crystal-Like Walls..."}],"publication":"Chemistry of Materials","doi":"10.1021/cm048453g","language":[{"iso":"eng"}],"article_type":"original","publication_status":"published","date_updated":"2023-03-09T09:00:44Z","publication_identifier":{"issn":["0897-4756","1520-5002"]},"author":[{"full_name":"Morell, Jürgen","first_name":"Jürgen","last_name":"Morell"},{"full_name":"Teixeira, Cilaine V.","first_name":"Cilaine V.","last_name":"Teixeira"},{"first_name":"Maximilian","last_name":"Cornelius","full_name":"Cornelius, Maximilian"},{"first_name":"Vivian","last_name":"Rebbin","full_name":"Rebbin, Vivian"},{"id":"23547","first_name":"Michael","orcid":"0000-0003-1711-2722","last_name":"Tiemann","full_name":"Tiemann, Michael"},{"full_name":"Amenitsch, Heinz","last_name":"Amenitsch","first_name":"Heinz"},{"full_name":"Fröba, Michael","first_name":"Michael","last_name":"Fröba"},{"full_name":"Lindén, Mika","first_name":"Mika","last_name":"Lindén"}],"title":"In situ Synchrotron SAXS/XRD Study on the Formation of Ordered Mesoscopic Hybrid Materials with Crystal-Like Walls","year":"2004","quality_controlled":"1","citation":{"mla":"Morell, Jürgen, et al. “In Situ Synchrotron SAXS/XRD Study on the Formation of Ordered Mesoscopic Hybrid Materials with Crystal-Like Walls.” <i>Chemistry of Materials</i>, 2004, pp. 5564–66, doi:<a href=\"https://doi.org/10.1021/cm048453g\">10.1021/cm048453g</a>.","bibtex":"@article{Morell_Teixeira_Cornelius_Rebbin_Tiemann_Amenitsch_Fröba_Lindén_2004, title={In situ Synchrotron SAXS/XRD Study on the Formation of Ordered Mesoscopic Hybrid Materials with Crystal-Like Walls}, DOI={<a href=\"https://doi.org/10.1021/cm048453g\">10.1021/cm048453g</a>}, journal={Chemistry of Materials}, author={Morell, Jürgen and Teixeira, Cilaine V. and Cornelius, Maximilian and Rebbin, Vivian and Tiemann, Michael and Amenitsch, Heinz and Fröba, Michael and Lindén, Mika}, year={2004}, pages={5564–5566} }","ama":"Morell J, Teixeira CV, Cornelius M, et al. In situ Synchrotron SAXS/XRD Study on the Formation of Ordered Mesoscopic Hybrid Materials with Crystal-Like Walls. <i>Chemistry of Materials</i>. Published online 2004:5564-5566. doi:<a href=\"https://doi.org/10.1021/cm048453g\">10.1021/cm048453g</a>","ieee":"J. Morell <i>et al.</i>, “In situ Synchrotron SAXS/XRD Study on the Formation of Ordered Mesoscopic Hybrid Materials with Crystal-Like Walls,” <i>Chemistry of Materials</i>, pp. 5564–5566, 2004, doi: <a href=\"https://doi.org/10.1021/cm048453g\">10.1021/cm048453g</a>.","apa":"Morell, J., Teixeira, C. V., Cornelius, M., Rebbin, V., Tiemann, M., Amenitsch, H., Fröba, M., &#38; Lindén, M. (2004). In situ Synchrotron SAXS/XRD Study on the Formation of Ordered Mesoscopic Hybrid Materials with Crystal-Like Walls. <i>Chemistry of Materials</i>, 5564–5566. <a href=\"https://doi.org/10.1021/cm048453g\">https://doi.org/10.1021/cm048453g</a>","short":"J. Morell, C.V. Teixeira, M. Cornelius, V. Rebbin, M. Tiemann, H. Amenitsch, M. Fröba, M. Lindén, Chemistry of Materials (2004) 5564–5566.","chicago":"Morell, Jürgen, Cilaine V. Teixeira, Maximilian Cornelius, Vivian Rebbin, Michael Tiemann, Heinz Amenitsch, Michael Fröba, and Mika Lindén. “In Situ Synchrotron SAXS/XRD Study on the Formation of Ordered Mesoscopic Hybrid Materials with Crystal-Like Walls.” <i>Chemistry of Materials</i>, 2004, 5564–66. <a href=\"https://doi.org/10.1021/cm048453g\">https://doi.org/10.1021/cm048453g</a>."},"user_id":"23547","_id":"25996","page":"5564-5566","status":"public"},{"citation":{"ama":"Tiemann M, Fröba M. Recent Advances in the Synthesis of Mesostructured Aluminum Phosphates. In: <i>Host‐Guest‐Systems Based on Nanoporous Crystals</i>. ; 2003. doi:<a href=\"https://doi.org/10.1002/3527602674.ch10\">10.1002/3527602674.ch10</a>","bibtex":"@inbook{Tiemann_Fröba_2003, title={Recent Advances in the Synthesis of Mesostructured Aluminum Phosphates}, DOI={<a href=\"https://doi.org/10.1002/3527602674.ch10\">10.1002/3527602674.ch10</a>}, booktitle={Host‐Guest‐Systems Based on Nanoporous Crystals}, author={Tiemann, Michael and Fröba, Michael}, year={2003} }","mla":"Tiemann, Michael, and Michael Fröba. “Recent Advances in the Synthesis of Mesostructured Aluminum Phosphates.” <i>Host‐Guest‐Systems Based on Nanoporous Crystals</i>, 2003, doi:<a href=\"https://doi.org/10.1002/3527602674.ch10\">10.1002/3527602674.ch10</a>.","short":"M. Tiemann, M. Fröba, in: Host‐Guest‐Systems Based on Nanoporous Crystals, 2003.","chicago":"Tiemann, Michael, and Michael Fröba. “Recent Advances in the Synthesis of Mesostructured Aluminum Phosphates.” In <i>Host‐Guest‐Systems Based on Nanoporous Crystals</i>, 2003. <a href=\"https://doi.org/10.1002/3527602674.ch10\">https://doi.org/10.1002/3527602674.ch10</a>.","apa":"Tiemann, M., &#38; Fröba, M. (2003). Recent Advances in the Synthesis of Mesostructured Aluminum Phosphates. In <i>Host‐Guest‐Systems Based on Nanoporous Crystals</i>. <a href=\"https://doi.org/10.1002/3527602674.ch10\">https://doi.org/10.1002/3527602674.ch10</a>","ieee":"M. Tiemann and M. Fröba, “Recent Advances in the Synthesis of Mesostructured Aluminum Phosphates,” in <i>Host‐Guest‐Systems Based on Nanoporous Crystals</i>, 2003."},"publication":"Host‐Guest‐Systems Based on Nanoporous Crystals","extern":"1","quality_controlled":"1","abstract":[{"lang":"eng","text":"Recent Advances in the Synthesis of Mesostructured Aluminium Phosphates..."}],"date_created":"2021-10-09T09:50:07Z","department":[{"_id":"35"},{"_id":"2"},{"_id":"307"}],"type":"book_chapter","author":[{"id":"23547","full_name":"Tiemann, Michael","last_name":"Tiemann","orcid":"0000-0003-1711-2722","first_name":"Michael"},{"last_name":"Fröba","first_name":"Michael","full_name":"Fröba, Michael"}],"title":"Recent Advances in the Synthesis of Mesostructured Aluminum Phosphates","year":"2003","status":"public","publication_status":"published","date_updated":"2023-03-09T09:01:52Z","language":[{"iso":"eng"}],"_id":"25997","user_id":"23547","doi":"10.1002/3527602674.ch10"},{"status":"public","user_id":"23547","page":"10053-10057","_id":"25998","quality_controlled":"1","citation":{"bibtex":"@article{Tiemann_Goletto_Blum_Babonneau_Amenitsch_Lindén_2002, title={In-Situ SAXS Studies on the Formation of Silicate/Surfactant Mesophases with Solubilized Benzene under Acidic Conditions}, DOI={<a href=\"https://doi.org/10.1021/la026473w\">10.1021/la026473w</a>}, journal={Langmuir}, author={Tiemann, Michael and Goletto, Valérie and Blum, Raphaël and Babonneau, Florence and Amenitsch, Heinz and Lindén, Mika}, year={2002}, pages={10053–10057} }","ama":"Tiemann M, Goletto V, Blum R, Babonneau F, Amenitsch H, Lindén M. In-Situ SAXS Studies on the Formation of Silicate/Surfactant Mesophases with Solubilized Benzene under Acidic Conditions. <i>Langmuir</i>. Published online 2002:10053-10057. doi:<a href=\"https://doi.org/10.1021/la026473w\">10.1021/la026473w</a>","mla":"Tiemann, Michael, et al. “In-Situ SAXS Studies on the Formation of Silicate/Surfactant Mesophases with Solubilized Benzene under Acidic Conditions.” <i>Langmuir</i>, 2002, pp. 10053–57, doi:<a href=\"https://doi.org/10.1021/la026473w\">10.1021/la026473w</a>.","short":"M. Tiemann, V. Goletto, R. Blum, F. Babonneau, H. Amenitsch, M. Lindén, Langmuir (2002) 10053–10057.","chicago":"Tiemann, Michael, Valérie Goletto, Raphaël Blum, Florence Babonneau, Heinz Amenitsch, and Mika Lindén. “In-Situ SAXS Studies on the Formation of Silicate/Surfactant Mesophases with Solubilized Benzene under Acidic Conditions.” <i>Langmuir</i>, 2002, 10053–57. <a href=\"https://doi.org/10.1021/la026473w\">https://doi.org/10.1021/la026473w</a>.","ieee":"M. Tiemann, V. Goletto, R. Blum, F. Babonneau, H. Amenitsch, and M. Lindén, “In-Situ SAXS Studies on the Formation of Silicate/Surfactant Mesophases with Solubilized Benzene under Acidic Conditions,” <i>Langmuir</i>, pp. 10053–10057, 2002, doi: <a href=\"https://doi.org/10.1021/la026473w\">10.1021/la026473w</a>.","apa":"Tiemann, M., Goletto, V., Blum, R., Babonneau, F., Amenitsch, H., &#38; Lindén, M. (2002). In-Situ SAXS Studies on the Formation of Silicate/Surfactant Mesophases with Solubilized Benzene under Acidic Conditions. <i>Langmuir</i>, 10053–10057. <a href=\"https://doi.org/10.1021/la026473w\">https://doi.org/10.1021/la026473w</a>"},"date_updated":"2023-03-09T09:02:25Z","publication_status":"published","article_type":"original","title":"In-Situ SAXS Studies on the Formation of Silicate/Surfactant Mesophases with Solubilized Benzene under Acidic Conditions","year":"2002","author":[{"id":"23547","full_name":"Tiemann, Michael","orcid":"0000-0003-1711-2722","first_name":"Michael","last_name":"Tiemann"},{"last_name":"Goletto","first_name":"Valérie","full_name":"Goletto, Valérie"},{"first_name":"Raphaël","last_name":"Blum","full_name":"Blum, Raphaël"},{"first_name":"Florence","last_name":"Babonneau","full_name":"Babonneau, Florence"},{"first_name":"Heinz","last_name":"Amenitsch","full_name":"Amenitsch, Heinz"},{"last_name":"Lindén","first_name":"Mika","full_name":"Lindén, Mika"}],"publication_identifier":{"issn":["0743-7463","1520-5827"]},"doi":"10.1021/la026473w","language":[{"iso":"eng"}],"abstract":[{"text":"The formation of mesoscopically ordered silica/surfactant composites under acidic synthesis conditions is studied by time-resolved in-situ small-angle X-ray scattering (SAXS) using synchrotron radiation. Benzene is used a an additive which acts as a weak swelling agent although most of the benzene molecules are found to reside near the surfactant/silicate interface region rather than in the micelle cores. With increasing relative amounts of benzene, the curvature of the micellar aggregates decreases, which finally leads to a transition from (hexagonally) rodlike to lamellar; a mechanism for this change in curvature is suggested.","lang":"eng"}],"extern":"1","publication":"Langmuir","type":"journal_article","department":[{"_id":"35"},{"_id":"2"},{"_id":"307"}],"date_created":"2021-10-09T09:50:51Z"},{"extern":"1","abstract":[{"lang":"eng","text":"Mesoporous aluminophosphates with a strict ratio of Al∶P = 1∶1 have been synthesised from a single-source molecular precursor."}],"publication":"Chemical Communications","type":"journal_article","department":[{"_id":"35"},{"_id":"2"},{"_id":"307"}],"date_created":"2021-10-09T10:04:05Z","publication_status":"published","date_updated":"2023-03-09T09:03:25Z","article_type":"original","title":"Mesoporous aluminophosphates from a single-source precursor","year":"2002","publication_identifier":{"issn":["1359-7345","1364-548X"]},"author":[{"id":"23547","orcid":"0000-0003-1711-2722","last_name":"Tiemann","first_name":"Michael","full_name":"Tiemann, Michael"},{"full_name":"Fröba, Michael","last_name":"Fröba","first_name":"Michael"}],"doi":"10.1039/b110662g","language":[{"iso":"eng"}],"quality_controlled":"1","citation":{"mla":"Tiemann, Michael, and Michael Fröba. “Mesoporous Aluminophosphates from a Single-Source Precursor.” <i>Chemical Communications</i>, 2002, pp. 406–07, doi:<a href=\"https://doi.org/10.1039/b110662g\">10.1039/b110662g</a>.","bibtex":"@article{Tiemann_Fröba_2002, title={Mesoporous aluminophosphates from a single-source precursor}, DOI={<a href=\"https://doi.org/10.1039/b110662g\">10.1039/b110662g</a>}, journal={Chemical Communications}, author={Tiemann, Michael and Fröba, Michael}, year={2002}, pages={406–407} }","ama":"Tiemann M, Fröba M. Mesoporous aluminophosphates from a single-source precursor. <i>Chemical Communications</i>. Published online 2002:406-407. doi:<a href=\"https://doi.org/10.1039/b110662g\">10.1039/b110662g</a>","ieee":"M. Tiemann and M. Fröba, “Mesoporous aluminophosphates from a single-source precursor,” <i>Chemical Communications</i>, pp. 406–407, 2002, doi: <a href=\"https://doi.org/10.1039/b110662g\">10.1039/b110662g</a>.","apa":"Tiemann, M., &#38; Fröba, M. (2002). Mesoporous aluminophosphates from a single-source precursor. <i>Chemical Communications</i>, 406–407. <a href=\"https://doi.org/10.1039/b110662g\">https://doi.org/10.1039/b110662g</a>","short":"M. Tiemann, M. Fröba, Chemical Communications (2002) 406–407.","chicago":"Tiemann, Michael, and Michael Fröba. “Mesoporous Aluminophosphates from a Single-Source Precursor.” <i>Chemical Communications</i>, 2002, 406–7. <a href=\"https://doi.org/10.1039/b110662g\">https://doi.org/10.1039/b110662g</a>."},"status":"public","user_id":"23547","page":"406-407","_id":"26001"},{"year":"2002","title":"Phase Behaviour of the System Triethanolamine-Decanoic Acid-Water","author":[{"last_name":"Backlund","first_name":"Sune","full_name":"Backlund, Sune"},{"last_name":"Friman","first_name":"Rauno","full_name":"Friman, Rauno"},{"full_name":"Karlsson, Stefan","first_name":"Stefan","last_name":"Karlsson"},{"full_name":"Tiemann, Michael","orcid":"0000-0003-1711-2722","last_name":"Tiemann","first_name":"Michael","id":"23547"}],"date_updated":"2023-03-09T09:05:27Z","article_type":"original","intvolume":"        39","language":[{"iso":"eng"}],"publication":"Tenside Surfactants Detergents","issue":"5","extern":"1","abstract":[{"text":"Phase Behaviour of the System Triethanolamine-Decanoic Acid-Water...","lang":"eng"}],"date_created":"2021-10-09T10:03:07Z","type":"journal_article","department":[{"_id":"35"},{"_id":"2"},{"_id":"307"}],"status":"public","page":"136-140","_id":"26000","user_id":"23547","volume":39,"citation":{"mla":"Backlund, Sune, et al. “Phase Behaviour of the System Triethanolamine-Decanoic Acid-Water.” <i>Tenside Surfactants Detergents</i>, vol. 39, no. 5, 2002, pp. 136–40.","bibtex":"@article{Backlund_Friman_Karlsson_Tiemann_2002, title={Phase Behaviour of the System Triethanolamine-Decanoic Acid-Water}, volume={39}, number={5}, journal={Tenside Surfactants Detergents}, author={Backlund, Sune and Friman, Rauno and Karlsson, Stefan and Tiemann, Michael}, year={2002}, pages={136–140} }","ama":"Backlund S, Friman R, Karlsson S, Tiemann M. Phase Behaviour of the System Triethanolamine-Decanoic Acid-Water. <i>Tenside Surfactants Detergents</i>. 2002;39(5):136-140.","ieee":"S. Backlund, R. Friman, S. Karlsson, and M. Tiemann, “Phase Behaviour of the System Triethanolamine-Decanoic Acid-Water,” <i>Tenside Surfactants Detergents</i>, vol. 39, no. 5, pp. 136–140, 2002.","apa":"Backlund, S., Friman, R., Karlsson, S., &#38; Tiemann, M. (2002). Phase Behaviour of the System Triethanolamine-Decanoic Acid-Water. <i>Tenside Surfactants Detergents</i>, <i>39</i>(5), 136–140.","short":"S. Backlund, R. Friman, S. Karlsson, M. Tiemann, Tenside Surfactants Detergents 39 (2002) 136–140.","chicago":"Backlund, Sune, Rauno Friman, Stefan Karlsson, and Michael Tiemann. “Phase Behaviour of the System Triethanolamine-Decanoic Acid-Water.” <i>Tenside Surfactants Detergents</i> 39, no. 5 (2002): 136–40."},"quality_controlled":"1"},{"citation":{"ama":"Tiemann M, Schulz M, Jäger C, Fröba M. Mesoporous Aluminophosphate Molecular Sieves Synthesized under Nonaqueous Conditions. <i>Chemistry of Materials</i>. Published online 2001:2885-2891. doi:<a href=\"https://doi.org/10.1021/cm011044p\">10.1021/cm011044p</a>","bibtex":"@article{Tiemann_Schulz_Jäger_Fröba_2001, title={Mesoporous Aluminophosphate Molecular Sieves Synthesized under Nonaqueous Conditions}, DOI={<a href=\"https://doi.org/10.1021/cm011044p\">10.1021/cm011044p</a>}, journal={Chemistry of Materials}, author={Tiemann, Michael and Schulz, Marcus and Jäger, Christian and Fröba, Michael}, year={2001}, pages={2885–2891} }","mla":"Tiemann, Michael, et al. “Mesoporous Aluminophosphate Molecular Sieves Synthesized under Nonaqueous Conditions.” <i>Chemistry of Materials</i>, 2001, pp. 2885–91, doi:<a href=\"https://doi.org/10.1021/cm011044p\">10.1021/cm011044p</a>.","chicago":"Tiemann, Michael, Marcus Schulz, Christian Jäger, and Michael Fröba. “Mesoporous Aluminophosphate Molecular Sieves Synthesized under Nonaqueous Conditions.” <i>Chemistry of Materials</i>, 2001, 2885–91. <a href=\"https://doi.org/10.1021/cm011044p\">https://doi.org/10.1021/cm011044p</a>.","short":"M. Tiemann, M. Schulz, C. Jäger, M. Fröba, Chemistry of Materials (2001) 2885–2891.","apa":"Tiemann, M., Schulz, M., Jäger, C., &#38; Fröba, M. (2001). Mesoporous Aluminophosphate Molecular Sieves Synthesized under Nonaqueous Conditions. <i>Chemistry of Materials</i>, 2885–2891. <a href=\"https://doi.org/10.1021/cm011044p\">https://doi.org/10.1021/cm011044p</a>","ieee":"M. Tiemann, M. Schulz, C. Jäger, and M. Fröba, “Mesoporous Aluminophosphate Molecular Sieves Synthesized under Nonaqueous Conditions,” <i>Chemistry of Materials</i>, pp. 2885–2891, 2001, doi: <a href=\"https://doi.org/10.1021/cm011044p\">10.1021/cm011044p</a>."},"quality_controlled":"1","_id":"26003","page":"2885-2891","user_id":"23547","status":"public","date_created":"2021-10-09T10:05:36Z","department":[{"_id":"35"},{"_id":"2"},{"_id":"307"}],"type":"journal_article","publication":"Chemistry of Materials","abstract":[{"lang":"eng","text":"Long-chain n-alkylamine surfactants have been used as structure-directing agents in the synthesis of mesoporous aluminophosphates by a highly cooperative formation mechanism in an alcoholic system. Small amounts of water in the synthesis mixture play a significant role in the hydrolysis of the aluminum precursor (Al[OiPr]3) and are important for the quality of the mesostructured products. The materials exhibit disordered mesostructures, the stability and structural order of which can be improved by a postsynthetic thermal treatment. The products are then stable enough for the removal of the surfactant molecules by acidic solvent extraction, yielding surface areas up to 690 m2/g."}],"extern":"1","language":[{"iso":"eng"}],"doi":"10.1021/cm011044p","publication_identifier":{"issn":["0897-4756","1520-5002"]},"author":[{"full_name":"Tiemann, Michael","orcid":"0000-0003-1711-2722","first_name":"Michael","last_name":"Tiemann","id":"23547"},{"full_name":"Schulz, Marcus","first_name":"Marcus","last_name":"Schulz"},{"last_name":"Jäger","first_name":"Christian","full_name":"Jäger, Christian"},{"full_name":"Fröba, Michael","first_name":"Michael","last_name":"Fröba"}],"year":"2001","title":"Mesoporous Aluminophosphate Molecular Sieves Synthesized under Nonaqueous Conditions","article_type":"original","date_updated":"2023-03-09T09:10:39Z","publication_status":"published"},{"citation":{"apa":"Tiemann, M., &#38; Fröba, M. (2001). Mesostructured Aluminophosphates Synthesized with Supramolecular Structure Directors. <i>Chemistry of Materials</i>, 3211–3217. <a href=\"https://doi.org/10.1021/cm0110371\">https://doi.org/10.1021/cm0110371</a>","ieee":"M. Tiemann and M. Fröba, “Mesostructured Aluminophosphates Synthesized with Supramolecular Structure Directors,” <i>Chemistry of Materials</i>, pp. 3211–3217, 2001, doi: <a href=\"https://doi.org/10.1021/cm0110371\">10.1021/cm0110371</a>.","short":"M. Tiemann, M. Fröba, Chemistry of Materials (2001) 3211–3217.","chicago":"Tiemann, Michael, and Michael Fröba. “Mesostructured Aluminophosphates Synthesized with Supramolecular Structure Directors.” <i>Chemistry of Materials</i>, 2001, 3211–17. <a href=\"https://doi.org/10.1021/cm0110371\">https://doi.org/10.1021/cm0110371</a>.","mla":"Tiemann, Michael, and Michael Fröba. “Mesostructured Aluminophosphates Synthesized with Supramolecular Structure Directors.” <i>Chemistry of Materials</i>, 2001, pp. 3211–17, doi:<a href=\"https://doi.org/10.1021/cm0110371\">10.1021/cm0110371</a>.","ama":"Tiemann M, Fröba M. Mesostructured Aluminophosphates Synthesized with Supramolecular Structure Directors. <i>Chemistry of Materials</i>. Published online 2001:3211-3217. doi:<a href=\"https://doi.org/10.1021/cm0110371\">10.1021/cm0110371</a>","bibtex":"@article{Tiemann_Fröba_2001, title={Mesostructured Aluminophosphates Synthesized with Supramolecular Structure Directors}, DOI={<a href=\"https://doi.org/10.1021/cm0110371\">10.1021/cm0110371</a>}, journal={Chemistry of Materials}, author={Tiemann, Michael and Fröba, Michael}, year={2001}, pages={3211–3217} }"},"quality_controlled":"1","_id":"26002","page":"3211-3217","user_id":"23547","status":"public","date_created":"2021-10-09T10:04:55Z","department":[{"_id":"35"},{"_id":"2"},{"_id":"307"}],"type":"journal_article","publication":"Chemistry of Materials","abstract":[{"text":"Over the past few years a growing number of scientists have dedicated their attention to the synthesis of mesostructured aluminophosphates following the concept of supramolecular structure direction. Their research has produced a large variety of synthetic approaches and yielded materials with various structural properties. Today a substantial number of publications have accumulated; this short review provides a general summary of the literature with the aim to display the opportunities for future work.","lang":"eng"}],"extern":"1","language":[{"iso":"eng"}],"doi":"10.1021/cm0110371","author":[{"id":"23547","full_name":"Tiemann, Michael","first_name":"Michael","last_name":"Tiemann","orcid":"0000-0003-1711-2722"},{"first_name":"Michael","last_name":"Fröba","full_name":"Fröba, Michael"}],"publication_identifier":{"issn":["0897-4756","1520-5002"]},"title":"Mesostructured Aluminophosphates Synthesized with Supramolecular Structure Directors","year":"2001","article_type":"original","date_updated":"2023-03-09T09:10:59Z","publication_status":"published"},{"user_id":"23547","page":"1342-1348","_id":"26005","status":"public","quality_controlled":"1","citation":{"apa":"Tiemann, M., Fröba, M., Rapp, G., &#38; Funari, S. S. (2000). Nonaqueous Synthesis of Mesostructured Aluminophosphate/Surfactant Composites:  Synthesis, Characterization, and In-Situ SAXS Studies. <i>Chemistry of Materials</i>, 1342–1348. <a href=\"https://doi.org/10.1021/cm991165d\">https://doi.org/10.1021/cm991165d</a>","ieee":"M. Tiemann, M. Fröba, G. Rapp, and S. S. Funari, “Nonaqueous Synthesis of Mesostructured Aluminophosphate/Surfactant Composites:  Synthesis, Characterization, and In-Situ SAXS Studies,” <i>Chemistry of Materials</i>, pp. 1342–1348, 2000, doi: <a href=\"https://doi.org/10.1021/cm991165d\">10.1021/cm991165d</a>.","short":"M. Tiemann, M. Fröba, G. Rapp, S.S. Funari, Chemistry of Materials (2000) 1342–1348.","chicago":"Tiemann, Michael, M. Fröba, G. Rapp, and S. S. Funari. “Nonaqueous Synthesis of Mesostructured Aluminophosphate/Surfactant Composites:  Synthesis, Characterization, and In-Situ SAXS Studies.” <i>Chemistry of Materials</i>, 2000, 1342–48. <a href=\"https://doi.org/10.1021/cm991165d\">https://doi.org/10.1021/cm991165d</a>.","mla":"Tiemann, Michael, et al. “Nonaqueous Synthesis of Mesostructured Aluminophosphate/Surfactant Composites:  Synthesis, Characterization, and In-Situ SAXS Studies.” <i>Chemistry of Materials</i>, 2000, pp. 1342–48, doi:<a href=\"https://doi.org/10.1021/cm991165d\">10.1021/cm991165d</a>.","ama":"Tiemann M, Fröba M, Rapp G, Funari SS. Nonaqueous Synthesis of Mesostructured Aluminophosphate/Surfactant Composites:  Synthesis, Characterization, and In-Situ SAXS Studies. <i>Chemistry of Materials</i>. Published online 2000:1342-1348. doi:<a href=\"https://doi.org/10.1021/cm991165d\">10.1021/cm991165d</a>","bibtex":"@article{Tiemann_Fröba_Rapp_Funari_2000, title={Nonaqueous Synthesis of Mesostructured Aluminophosphate/Surfactant Composites:  Synthesis, Characterization, and In-Situ SAXS Studies}, DOI={<a href=\"https://doi.org/10.1021/cm991165d\">10.1021/cm991165d</a>}, journal={Chemistry of Materials}, author={Tiemann, Michael and Fröba, M. and Rapp, G. and Funari, S. S.}, year={2000}, pages={1342–1348} }"},"doi":"10.1021/cm991165d","language":[{"iso":"eng"}],"publication_status":"published","date_updated":"2023-03-09T09:09:05Z","article_type":"original","title":"Nonaqueous Synthesis of Mesostructured Aluminophosphate/Surfactant Composites:  Synthesis, Characterization, and In-Situ SAXS Studies","year":"2000","publication_identifier":{"issn":["0897-4756","1520-5002"]},"author":[{"id":"23547","full_name":"Tiemann, Michael","first_name":"Michael","orcid":"0000-0003-1711-2722","last_name":"Tiemann"},{"last_name":"Fröba","first_name":"M.","full_name":"Fröba, M."},{"first_name":"G.","last_name":"Rapp","full_name":"Rapp, G."},{"full_name":"Funari, S. S.","last_name":"Funari","first_name":"S. S."}],"type":"journal_article","department":[{"_id":"35"},{"_id":"2"},{"_id":"307"}],"date_created":"2021-10-09T10:06:55Z","extern":"1","abstract":[{"text":"Mesostructured aluminophosphate/dodecyl phosphate composite materials were synthesized under aqueous and alcoholic conditions. The syntheses were monitored by temperature- and time-resolved in-situ small-angle X-ray scattering (SAXS). In the aqueous synthesis, a lamellar mesostructure is formed within the first few minutes of the reaction; this structure maintains a constant d spacing independent of the reaction time and temperature. The alcoholic synthesis at low temperature yields a mixture of a lamellar and a supposedly inverted hexagonal mesostructure. SAXS investigations show that these two phases evolve competitively. The lamellar structure is favored by higher temperatures and/or longer synthesis times; above ∼70 °C it is formed exclusively. Mixtures of both phases can be isolated as solid materials, but thermal analysis shows that the inverted hexagonal product transforms into the lamellar phase at ∼35−43 °C. The alcoholic synthesis is a highly cooperative reaction; the pure surfactant/alcohol systems are not lyotropic as long as the inorganic reactants are absent. In comparison, the surfactant/water system with the same surfactant concentrations as employed for the aqueous syntheses is lyotropic with a lamellar structure.","lang":"eng"}],"publication":"Chemistry of Materials"},{"type":"journal_article","department":[{"_id":"35"},{"_id":"2"},{"_id":"307"}],"date_created":"2021-10-09T10:06:12Z","extern":"1","abstract":[{"lang":"eng","text":"The atomic structure of ordered mesostructured aluminophosphates with dodecyl phosphate as the structure-directing template was investigated by multinuclear solid-state NMR. Two different types of materials were studied:  one with the template headgroup as the only phosphate source and one where additionally phosphoric acid was used in the synthesis. All 31P and 27Al NMR resonances can be subdivided into three groups depending on the sample composition. Furthermore, 2D heteronuclear correlation NMR measurements allow a conclusive and unambiguous identification of the phosphate headgroup resonances of the template molecules and the determination of water and/or hydroxyl units. Most notably, there is an obvious correlation between the d001 values of the samples as measured by powder X-ray diffraction and the appearance of the various groups of 27Al and 31P resonances."}],"publication":"The Journal of Physical Chemistry B","doi":"10.1021/jp000337n","language":[{"iso":"eng"}],"publication_status":"published","date_updated":"2023-03-09T09:09:47Z","article_type":"original","title":"NMR Characterization of Mesostructured Aluminophosphates","year":"2000","publication_identifier":{"issn":["1520-6106","1520-5207"]},"author":[{"full_name":"Schulz, M.","first_name":"M.","last_name":"Schulz"},{"first_name":"Michael","last_name":"Tiemann","orcid":"0000-0003-1711-2722","full_name":"Tiemann, Michael","id":"23547"},{"last_name":"Fröba","first_name":"M.","full_name":"Fröba, M."},{"full_name":"Jäger, C.","first_name":"C.","last_name":"Jäger"}],"quality_controlled":"1","citation":{"mla":"Schulz, M., et al. “NMR Characterization of Mesostructured Aluminophosphates.” <i>The Journal of Physical Chemistry B</i>, 2000, pp. 10473–81, doi:<a href=\"https://doi.org/10.1021/jp000337n\">10.1021/jp000337n</a>.","bibtex":"@article{Schulz_Tiemann_Fröba_Jäger_2000, title={NMR Characterization of Mesostructured Aluminophosphates}, DOI={<a href=\"https://doi.org/10.1021/jp000337n\">10.1021/jp000337n</a>}, journal={The Journal of Physical Chemistry B}, author={Schulz, M. and Tiemann, Michael and Fröba, M. and Jäger, C.}, year={2000}, pages={10473–10481} }","ama":"Schulz M, Tiemann M, Fröba M, Jäger C. NMR Characterization of Mesostructured Aluminophosphates. <i>The Journal of Physical Chemistry B</i>. Published online 2000:10473-10481. doi:<a href=\"https://doi.org/10.1021/jp000337n\">10.1021/jp000337n</a>","ieee":"M. Schulz, M. Tiemann, M. Fröba, and C. Jäger, “NMR Characterization of Mesostructured Aluminophosphates,” <i>The Journal of Physical Chemistry B</i>, pp. 10473–10481, 2000, doi: <a href=\"https://doi.org/10.1021/jp000337n\">10.1021/jp000337n</a>.","apa":"Schulz, M., Tiemann, M., Fröba, M., &#38; Jäger, C. (2000). NMR Characterization of Mesostructured Aluminophosphates. <i>The Journal of Physical Chemistry B</i>, 10473–10481. <a href=\"https://doi.org/10.1021/jp000337n\">https://doi.org/10.1021/jp000337n</a>","short":"M. Schulz, M. Tiemann, M. Fröba, C. Jäger, The Journal of Physical Chemistry B (2000) 10473–10481.","chicago":"Schulz, M., Michael Tiemann, M. Fröba, and C. Jäger. “NMR Characterization of Mesostructured Aluminophosphates.” <i>The Journal of Physical Chemistry B</i>, 2000, 10473–81. <a href=\"https://doi.org/10.1021/jp000337n\">https://doi.org/10.1021/jp000337n</a>."},"user_id":"23547","page":"10473-10481","_id":"26004","status":"public"},{"citation":{"mla":"Tiemann, Michael, et al. “In-Situ Small Angle x-Ray Scattering (SAXS) Studies on the Formation of Mesostructured Aluminophosphate / Surfactant Composite Materials.” <i>Nanoporous Materials II, Proceedings of the 2nd Conference on Access in Nanoporous Materials</i>, 2000, doi:<a href=\"https://doi.org/10.1016/s0167-2991(00)80258-x\">10.1016/s0167-2991(00)80258-x</a>.","ama":"Tiemann M, Fröba M, Rapp G, Funari SS. In-situ small angle x-ray scattering (SAXS) studies on the formation of mesostructured aluminophosphate / surfactant composite materials. In: <i>Nanoporous Materials II, Proceedings of the 2nd Conference on Access in Nanoporous Materials</i>. ; 2000. doi:<a href=\"https://doi.org/10.1016/s0167-2991(00)80258-x\">10.1016/s0167-2991(00)80258-x</a>","bibtex":"@inbook{Tiemann_Fröba_Rapp_Funari_2000, title={In-situ small angle x-ray scattering (SAXS) studies on the formation of mesostructured aluminophosphate / surfactant composite materials}, DOI={<a href=\"https://doi.org/10.1016/s0167-2991(00)80258-x\">10.1016/s0167-2991(00)80258-x</a>}, booktitle={Nanoporous Materials II, Proceedings of the 2nd Conference on Access in Nanoporous Materials}, author={Tiemann, Michael and Fröba, M. and Rapp, G. and Funari, S.S.}, year={2000} }","apa":"Tiemann, M., Fröba, M., Rapp, G., &#38; Funari, S. S. (2000). In-situ small angle x-ray scattering (SAXS) studies on the formation of mesostructured aluminophosphate / surfactant composite materials. In <i>Nanoporous Materials II, Proceedings of the 2nd Conference on Access in Nanoporous Materials</i>. <a href=\"https://doi.org/10.1016/s0167-2991(00)80258-x\">https://doi.org/10.1016/s0167-2991(00)80258-x</a>","ieee":"M. Tiemann, M. Fröba, G. Rapp, and S. S. Funari, “In-situ small angle x-ray scattering (SAXS) studies on the formation of mesostructured aluminophosphate / surfactant composite materials,” in <i>Nanoporous Materials II, Proceedings of the 2nd Conference on Access in Nanoporous Materials</i>, 2000.","short":"M. Tiemann, M. Fröba, G. Rapp, S.S. Funari, in: Nanoporous Materials II, Proceedings of the 2nd Conference on Access in Nanoporous Materials, 2000.","chicago":"Tiemann, Michael, M. Fröba, G. Rapp, and S.S. Funari. “In-Situ Small Angle x-Ray Scattering (SAXS) Studies on the Formation of Mesostructured Aluminophosphate / Surfactant Composite Materials.” In <i>Nanoporous Materials II, Proceedings of the 2nd Conference on Access in Nanoporous Materials</i>, 2000. <a href=\"https://doi.org/10.1016/s0167-2991(00)80258-x\">https://doi.org/10.1016/s0167-2991(00)80258-x</a>."},"publication":"Nanoporous Materials II, Proceedings of the 2nd Conference on Access in Nanoporous Materials","abstract":[{"lang":"eng","text":"Mesostructured aluminophosphate / surfactant composite materials were prepared from aqueous and alcoholic systems. Syntheses in ethanol or methanol, respectively, lead to mixtures of two nanostructured phases. One of these consists of hexagonally arranged rod-like assemblies of the surfactant molecules with the head groups located in the centres, encapsulating the inorganic aluminophosphate; the other is lamellar. The syntheses were monitored by in-situ temperature- and time-resolved small angle X-ray scattering (SAXS)."}],"quality_controlled":"1","extern":"1","date_created":"2021-10-09T10:07:37Z","department":[{"_id":"35"},{"_id":"2"},{"_id":"307"}],"type":"book_chapter","publication_identifier":{"issn":["0167-2991"]},"author":[{"id":"23547","full_name":"Tiemann, Michael","last_name":"Tiemann","orcid":"0000-0003-1711-2722","first_name":"Michael"},{"first_name":"M.","last_name":"Fröba","full_name":"Fröba, M."},{"first_name":"G.","last_name":"Rapp","full_name":"Rapp, G."},{"last_name":"Funari","first_name":"S.S.","full_name":"Funari, S.S."}],"year":"2000","title":"In-situ small angle x-ray scattering (SAXS) studies on the formation of mesostructured aluminophosphate / surfactant composite materials","status":"public","date_updated":"2023-03-09T09:10:14Z","publication_status":"published","language":[{"iso":"eng"}],"_id":"26006","doi":"10.1016/s0167-2991(00)80258-x","user_id":"23547"},{"year":"1999","title":"Multiple K-edge XAS for the structural analysis of thiophenolate bridged heterotrinuclear complexes","author":[{"full_name":"Meyer-Klaucke, W.","last_name":"Meyer-Klaucke","first_name":"W."},{"last_name":"Glaser","first_name":"T.","full_name":"Glaser, T."},{"full_name":"Fröba, M.","last_name":"Fröba","first_name":"M."},{"full_name":"Tiemann, Michael","last_name":"Tiemann","orcid":"0000-0003-1711-2722","first_name":"Michael","id":"23547"},{"full_name":"Wong, J.","first_name":"J.","last_name":"Wong"},{"last_name":"Trautwein","first_name":"A. X.","full_name":"Trautwein, A. X."}],"publication_identifier":{"issn":["0909-0495"]},"publication_status":"published","date_updated":"2023-03-09T09:08:40Z","article_type":"original","language":[{"iso":"eng"}],"doi":"10.1107/s0909049598017804","publication":"Journal of Synchrotron Radiation","extern":"1","abstract":[{"lang":"eng","text":"Multiple K-edge XAS for the structural analysis of thiophenolate bridged heterotrinuclear complexes"}],"date_created":"2021-10-09T10:13:40Z","type":"journal_article","department":[{"_id":"35"},{"_id":"2"},{"_id":"307"}],"status":"public","page":"397-399","_id":"26008","user_id":"23547","citation":{"mla":"Meyer-Klaucke, W., et al. “Multiple K-Edge XAS for the Structural Analysis of Thiophenolate Bridged Heterotrinuclear Complexes.” <i>Journal of Synchrotron Radiation</i>, 1999, pp. 397–99, doi:<a href=\"https://doi.org/10.1107/s0909049598017804\">10.1107/s0909049598017804</a>.","ama":"Meyer-Klaucke W, Glaser T, Fröba M, Tiemann M, Wong J, Trautwein AX. Multiple K-edge XAS for the structural analysis of thiophenolate bridged heterotrinuclear complexes. <i>Journal of Synchrotron Radiation</i>. Published online 1999:397-399. doi:<a href=\"https://doi.org/10.1107/s0909049598017804\">10.1107/s0909049598017804</a>","bibtex":"@article{Meyer-Klaucke_Glaser_Fröba_Tiemann_Wong_Trautwein_1999, title={Multiple K-edge XAS for the structural analysis of thiophenolate bridged heterotrinuclear complexes}, DOI={<a href=\"https://doi.org/10.1107/s0909049598017804\">10.1107/s0909049598017804</a>}, journal={Journal of Synchrotron Radiation}, author={Meyer-Klaucke, W. and Glaser, T. and Fröba, M. and Tiemann, Michael and Wong, J. and Trautwein, A. X.}, year={1999}, pages={397–399} }","apa":"Meyer-Klaucke, W., Glaser, T., Fröba, M., Tiemann, M., Wong, J., &#38; Trautwein, A. X. (1999). Multiple K-edge XAS for the structural analysis of thiophenolate bridged heterotrinuclear complexes. <i>Journal of Synchrotron Radiation</i>, 397–399. <a href=\"https://doi.org/10.1107/s0909049598017804\">https://doi.org/10.1107/s0909049598017804</a>","ieee":"W. Meyer-Klaucke, T. Glaser, M. Fröba, M. Tiemann, J. Wong, and A. X. Trautwein, “Multiple K-edge XAS for the structural analysis of thiophenolate bridged heterotrinuclear complexes,” <i>Journal of Synchrotron Radiation</i>, pp. 397–399, 1999, doi: <a href=\"https://doi.org/10.1107/s0909049598017804\">10.1107/s0909049598017804</a>.","short":"W. Meyer-Klaucke, T. Glaser, M. Fröba, M. Tiemann, J. Wong, A.X. Trautwein, Journal of Synchrotron Radiation (1999) 397–399.","chicago":"Meyer-Klaucke, W., T. Glaser, M. Fröba, Michael Tiemann, J. Wong, and A. X. Trautwein. “Multiple K-Edge XAS for the Structural Analysis of Thiophenolate Bridged Heterotrinuclear Complexes.” <i>Journal of Synchrotron Radiation</i>, 1999, 397–99. <a href=\"https://doi.org/10.1107/s0909049598017804\">https://doi.org/10.1107/s0909049598017804</a>."},"quality_controlled":"1"},{"publication":"MRS Proceedings","citation":{"chicago":"Tiemann, Michael, M. Fröba, and J. Wong. “Synthesis and Al K-Edge Xanes Investigation of Mesostructured Aluminophosphates.” <i>MRS Proceedings</i>, 1999. <a href=\"https://doi.org/10.1557/proc-547-87\">https://doi.org/10.1557/proc-547-87</a>.","short":"M. Tiemann, M. Fröba, J. Wong, MRS Proceedings (1999).","apa":"Tiemann, M., Fröba, M., &#38; Wong, J. (1999). Synthesis and Al K-Edge Xanes Investigation of Mesostructured Aluminophosphates. <i>MRS Proceedings</i>. <a href=\"https://doi.org/10.1557/proc-547-87\">https://doi.org/10.1557/proc-547-87</a>","ieee":"M. Tiemann, M. Fröba, and J. Wong, “Synthesis and Al K-Edge Xanes Investigation of Mesostructured Aluminophosphates,” <i>MRS Proceedings</i>, 1999, doi: <a href=\"https://doi.org/10.1557/proc-547-87\">10.1557/proc-547-87</a>.","ama":"Tiemann M, Fröba M, Wong J. Synthesis and Al K-Edge Xanes Investigation of Mesostructured Aluminophosphates. <i>MRS Proceedings</i>. Published online 1999. doi:<a href=\"https://doi.org/10.1557/proc-547-87\">10.1557/proc-547-87</a>","bibtex":"@article{Tiemann_Fröba_Wong_1999, title={Synthesis and Al K-Edge Xanes Investigation of Mesostructured Aluminophosphates}, DOI={<a href=\"https://doi.org/10.1557/proc-547-87\">10.1557/proc-547-87</a>}, journal={MRS Proceedings}, author={Tiemann, Michael and Fröba, M. and Wong, J.}, year={1999} }","mla":"Tiemann, Michael, et al. “Synthesis and Al K-Edge Xanes Investigation of Mesostructured Aluminophosphates.” <i>MRS Proceedings</i>, 1999, doi:<a href=\"https://doi.org/10.1557/proc-547-87\">10.1557/proc-547-87</a>."},"extern":"1","abstract":[{"text":"We report on the synthesis of lamellar mesostructured aluminophosphate composites which contain variable relative amounts of aluminium oxide species in the core regions of the lamellae; this is investigated quantitatively by Al K-edge XANES spectroscopy. Templating is achieved by the utilisation of monododecyl phosphate surfactant. If no phosphorous source (such as H3PO4) is used for the synthesis, the phosphate head groups of the surfactant become incorporated into the inorganic network to form similar lamellar aluminophosphate structures. Thus, the surfactant serves as both template and reactant.","lang":"eng"}],"quality_controlled":"1","date_created":"2021-10-09T10:12:51Z","type":"journal_article","department":[{"_id":"35"},{"_id":"2"},{"_id":"307"}],"status":"public","title":"Synthesis and Al K-Edge Xanes Investigation of Mesostructured Aluminophosphates","year":"1999","publication_identifier":{"issn":["0272-9172","1946-4274"]},"author":[{"orcid":"0000-0003-1711-2722","last_name":"Tiemann","first_name":"Michael","full_name":"Tiemann, Michael","id":"23547"},{"full_name":"Fröba, M.","last_name":"Fröba","first_name":"M."},{"first_name":"J.","last_name":"Wong","full_name":"Wong, J."}],"publication_status":"published","date_updated":"2023-03-09T09:08:01Z","article_type":"original","language":[{"iso":"eng"}],"_id":"26007","user_id":"23547","doi":"10.1557/proc-547-87"},{"_id":"26009","page":"3475-3483","user_id":"23547","status":"public","citation":{"short":"M. Fröba, M. Tiemann, Chemistry of Materials (1998) 3475–3483.","chicago":"Fröba, Michael, and Michael Tiemann. “A New Role of the Surfactant in the Synthesis of Mesostructured Phases:  Dodecyl Phosphate as Template and Reactant for Aluminophosphates.” <i>Chemistry of Materials</i>, 1998, 3475–83. <a href=\"https://doi.org/10.1021/cm980712c\">https://doi.org/10.1021/cm980712c</a>.","apa":"Fröba, M., &#38; Tiemann, M. (1998). A New Role of the Surfactant in the Synthesis of Mesostructured Phases:  Dodecyl Phosphate as Template and Reactant for Aluminophosphates. <i>Chemistry of Materials</i>, 3475–3483. <a href=\"https://doi.org/10.1021/cm980712c\">https://doi.org/10.1021/cm980712c</a>","ieee":"M. Fröba and M. Tiemann, “A New Role of the Surfactant in the Synthesis of Mesostructured Phases:  Dodecyl Phosphate as Template and Reactant for Aluminophosphates,” <i>Chemistry of Materials</i>, pp. 3475–3483, 1998, doi: <a href=\"https://doi.org/10.1021/cm980712c\">10.1021/cm980712c</a>.","ama":"Fröba M, Tiemann M. A New Role of the Surfactant in the Synthesis of Mesostructured Phases:  Dodecyl Phosphate as Template and Reactant for Aluminophosphates. <i>Chemistry of Materials</i>. Published online 1998:3475-3483. doi:<a href=\"https://doi.org/10.1021/cm980712c\">10.1021/cm980712c</a>","bibtex":"@article{Fröba_Tiemann_1998, title={A New Role of the Surfactant in the Synthesis of Mesostructured Phases:  Dodecyl Phosphate as Template and Reactant for Aluminophosphates}, DOI={<a href=\"https://doi.org/10.1021/cm980712c\">10.1021/cm980712c</a>}, journal={Chemistry of Materials}, author={Fröba, Michael and Tiemann, Michael}, year={1998}, pages={3475–3483} }","mla":"Fröba, Michael, and Michael Tiemann. “A New Role of the Surfactant in the Synthesis of Mesostructured Phases:  Dodecyl Phosphate as Template and Reactant for Aluminophosphates.” <i>Chemistry of Materials</i>, 1998, pp. 3475–83, doi:<a href=\"https://doi.org/10.1021/cm980712c\">10.1021/cm980712c</a>."},"quality_controlled":"1","language":[{"iso":"eng"}],"doi":"10.1021/cm980712c","publication_identifier":{"issn":["0897-4756","1520-5002"]},"author":[{"full_name":"Fröba, Michael","last_name":"Fröba","first_name":"Michael"},{"full_name":"Tiemann, Michael","first_name":"Michael","last_name":"Tiemann","orcid":"0000-0003-1711-2722","id":"23547"}],"year":"1998","title":"A New Role of the Surfactant in the Synthesis of Mesostructured Phases:  Dodecyl Phosphate as Template and Reactant for Aluminophosphates","article_type":"original","date_updated":"2023-03-09T09:07:28Z","publication_status":"published","date_created":"2021-10-09T10:14:44Z","department":[{"_id":"35"},{"_id":"163"},{"_id":"307"}],"type":"journal_article","publication":"Chemistry of Materials","abstract":[{"lang":"eng","text":"Lamellar mesostructured aluminophosphates were synthesized from aluminum triisopropoxide and phosphoric acid; monododecyl phosphate surfactant was used as structure-directing template. Depending on the relative Al/P ratio in the samples, variable relative amounts of tetrahedrally and octahedrally coordinated Al are found, indicating that both aluminophosphate and aluminum oxide species (as thermodynamically favored) are being formed in the syntheses. This is investigated quantitatively by Al K-edge XANES spectroscopy. The same syntheses were carried out without phosphoric acid, resulting in similar lamellar structures. The inorganic lamellae of these products consist to a significant extent of aluminophosphate rather than exclusively of aluminum oxide, which means that the phosphate headgroups of the surfactant molecules become incorporated into the inorganic network. Thus, for the first time, the surfactant serves as both template and reactant."}],"extern":"1"}]