@article{27509, abstract = {{ Purpose The currently existing restrictions regarding the deployment of additively manufactured components because of poor surface roughness, porosity and residual stresses as well as their influence on the low-cycle fatigue (LCF) strength are addressed in this paper. Design/methodology/approach This study aims to evaluating the effect of different pre- and post-treatments on the LCF strength of additively manufactured 316L parts. Therefore, 316L specimens manufactured by laser powder bed fusion were examined in their as-built state as well as after grinding, or coating with regard to the surface roughness, residual stresses and LCF strength. To differentiate between topographical effects and residual stress-related phenomena, stress-relieved 316L specimens served as a reference throughout the investigations. To enable an alumina coating of the 316L components, atmospheric plasma spraying was used, and the near-surface residual stresses and the surface roughness are measured and investigated. Findings The results have shown that the applied pre- and post-treatments such as stress-relief heat treatment, grinding and alumina coating have each led to an increase in LCF strength of the 316L specimens. In contrast, the non-heat-treated specimens predominantly exhibited coating delamination. Originality/value To the best of the authors’ knowledge, this is the first study of the correlation between the LCF behavior of additively manufactured uncoated 316L specimens in comparison with additively manufactured 316L specimens with an alumina coating. }}, author = {{Garthe, Kai-Uwe and Hoyer, Kay-Peter and Hagen, Leif and Tillmann, Wolfgang and Schaper, Mirko}}, issn = {{1355-2546}}, journal = {{Rapid Prototyping Journal}}, title = {{{Correlation between pre- and post-treatments of additively manufactured 316L parts and the resulting low cycle fatigue behavior}}}, doi = {{10.1108/rpj-01-2021-0017}}, year = {{2021}}, } @article{24087, abstract = {{Resorbable implants are highly beneficial to reduce patient burden since they need not be removed after a defined period. Currently, magnesium (Mg) and polymers are being applied as bioresorbable materials. However, for some applications the insufficient mechanical properties and high degradation rate of Mg cause the need for new materials. Iron (Fe)-based alloys are promising due to their biocompatibility and good mechanical properties, but their degradation rate is too low and needs to be adapted eg. via alloying with manganese (Mn). Besides, phases with high electrochemical potential lead to increased degradation of residual material with lower potential based on the galvanic coupling. Here, silver (Ag) is promising for the formation of such phases due to its high electrochemical potential (+0.8 V vs. SHE), immiscibility with Fe, biocompatibility, and anti-bacterial properties. Since remaining silver particles can lead to adverse consequences as thrombosis, these particles need to dissolve after the matrix material. Thus a silver alloy with high electrochemical potential, biocompatibility, and adjusted degradation behavior is required as an additive for iron-based bioresorbable materials. Several silver alloying systems are possible, but regarding the electrochemical potential and degradation behavior of binary alloys, calcium (Ca) and lanthanum (La) are best-suited considering their biocompatibility. Accordingly, this research addresses AgCa and AgCaLa alloys as additives for iron-based degradable materials with adapted degradation behavior.}}, author = {{Krüger, Jan Tobias and Hoyer, Kay-Peter and Filor, Viviane and Pramanik, Sudipta and Kietzmann, Manfred and Meißner, Jessica and Schaper, Mirko}}, issn = {{0925-8388}}, journal = {{Journal of Alloys and Compounds}}, title = {{{Novel AgCa and AgCaLa alloys for Fe-based bioresorbable implants with adapted degradation}}}, doi = {{10.1016/j.jallcom.2021.159544}}, year = {{2021}}, } @article{23897, author = {{Andreiev, Anatolii and Hoyer, Kay-Peter and Dula, Dimitri and Hengsbach, Florian and Grydin, Olexandr and Frolov, Yaroslav and Schaper, Mirko}}, issn = {{0921-5093}}, journal = {{Materials Science and Engineering: A}}, title = {{{Laser beam melting of functionally graded materials with application-adapted tailoring of magnetic and mechanical performance}}}, doi = {{10.1016/j.msea.2021.141662}}, year = {{2021}}, } @article{23911, author = {{Pramanik, Sudipta and Andreiev, Anatolii and Hoyer, Kay-Peter and Schaper, Mirko}}, issn = {{0142-1123}}, journal = {{International Journal of Fatigue}}, title = {{{Quasi in-situ analysis of fracture path during cyclic loading of double-edged U notched additively manufactured FeCo alloy}}}, doi = {{10.1016/j.ijfatigue.2021.106498}}, year = {{2021}}, } @article{24088, author = {{Pramanik, Sudipta and Tasche, Lennart and Hoyer, Kay-Peter and Schaper, Mirko}}, issn = {{2214-8604}}, journal = {{Additive Manufacturing}}, title = {{{Investigating the microstructure of an additively manufactured FeCo alloy: an electron microscopy study}}}, doi = {{10.1016/j.addma.2021.102087}}, year = {{2021}}, } @article{41508, author = {{Camberg, Alan Adam and Andreiev, Anatolii and Pramanik, Sudipta and Hoyer, Kay-Peter and Tröster, Thomas and Schaper, Mirko}}, issn = {{0921-5093}}, journal = {{Materials Science and Engineering: A}}, keywords = {{Mechanical Engineering, Mechanics of Materials, Condensed Matter Physics, General Materials Science}}, publisher = {{Elsevier BV}}, title = {{{Strength enhancement of AlMg sheet metal parts by rapid heating and subsequent cold die stamping of severely cold-rolled blanks}}}, doi = {{10.1016/j.msea.2021.142312}}, volume = {{831}}, year = {{2021}}, } @article{27700, author = {{Camberg, Alan Adam and Andreiev, Anatolii and Pramanik, Sudipta and Hoyer, Kay-Peter and Tröster, Thomas and Schaper, Mirko}}, issn = {{0921-5093}}, journal = {{Materials Science and Engineering: A}}, publisher = {{Elsevier}}, title = {{{Strength enhancement of AlMg sheet metal parts by rapid heating and subsequent cold die stamping of severely cold-rolled blanks}}}, doi = {{10.1016/j.msea.2021.142312}}, year = {{2021}}, } @article{23898, author = {{Andreiev, Anatolii and Hoyer, Kay-Peter and Dula, Dimitri and Hengsbach, Florian and Haase, Michael and Gierse, Jan and Zimmer, Detmar and Tröster, Thomas and Schaper, Mirko}}, issn = {{0924-0136}}, journal = {{Journal of Materials Processing Technology}}, title = {{{Soft-magnetic behavior of laser beam melted FeSi3 alloy with graded cross-section}}}, doi = {{10.1016/j.jmatprotec.2021.117183}}, year = {{2021}}, } @article{41519, abstract = {{AbstractDifferent studies have been demonstrated that the surface integrity of substrate bulk materials to be coated has a significant impact on the adhesion of thermally sprayed coatings. It is known that the surface integrity of parts processed by selective laser melting (SLM) differs from those obtained from bulk materials. Although 316L stainless steel is among the most investigated material for SLM, the adhesion of thermally sprayed coatings on 316L stainless steel substrates processed by SLM has not been studied yet. This study aims at evaluating the effect of various mechanical pre-treatments onto 316L stainless steel substrates processed by SLM and their effect on the adhesion of high velocity oxy-fuel (HVOF)-sprayed WC-Co coatings. To differentiate between topographical effects and residual stress-related phenomena, a stress-relief heat treatment of the SLM substrates served as a reference throughout the investigations. The differently pre-treated SLM substrates were investigated with regard to the surface roughness and residual stresses. For the HVOF-sprayed SLM composites, Vickers interfacial indentation tests were conducted to assess the resulting coating adhesion. The findings demonstrated that the HVOF-sprayed WC-Co coatings predominantly exhibit good adhesion to the SLM 316L substrates. However, it was found that the stress state in the SLM 316L substrate surface is more likely to affect the adhesion of the WC-Co coating, while the substrate surface roughness showed a marginal effect.}}, author = {{Tillmann, Wolfgang and Hagen, Leif and Schaak, Christoph and Liß, J. and Schaper, Mirko and Hoyer, Kay-Peter and Aydinöz, Mehmet Esat and Garthe, Kai-Uwe}}, issn = {{1059-9630}}, journal = {{Journal of Thermal Spray Technology}}, keywords = {{Materials Chemistry, Surfaces, Coatings and Films, Condensed Matter Physics}}, number = {{6}}, pages = {{1396--1409}}, publisher = {{Springer Science and Business Media LLC}}, title = {{{Adhesion of HVOF-Sprayed WC-Co Coatings on 316L Substrates Processed by SLM}}}, doi = {{10.1007/s11666-020-01081-y}}, volume = {{29}}, year = {{2020}}, } @article{41518, author = {{Tillmann, Wolfgang and Hagen, Leif and Garthe, Kai-Uwe and Hoyer, Kay-Peter and Schaper, Mirko}}, issn = {{0933-5137}}, journal = {{Materialwissenschaft und Werkstofftechnik}}, keywords = {{Mechanical Engineering, Mechanics of Materials, Condensed Matter Physics, General Materials Science}}, number = {{11}}, pages = {{1452--1464}}, publisher = {{Wiley}}, title = {{{Effect of substrate pre‐treatment on the low cycle fatigue performance of tungsten carbide‐cobalt coated additive manufactured 316 L substrates}}}, doi = {{10.1002/mawe.202000109}}, volume = {{51}}, year = {{2020}}, } @article{24100, abstract = {{Zinc oxide (ZnO) hollow spheres with defined morphology and micro-/nanostructure are prepared by a hydrothermal synthesis approach. The materials possess fine-leaved structures at their particle surface (nanowall hollow micro spheres). Morphology control is achieved by citric acid used as an additive in variable relative quantities during the synthesis. The structure formation is studied by various time-dependent ex situ methods, such as scanning electron microscopy, x-ray diffraction, and Raman spectroscopy. The fine-leaved surface structure is characterized by high-resolution transmission electron microscopy techniques (HRTEM, STEM), using a high-angle annular dark field detector, as well as by differential phase contrast analysis. In-depth structural characterization of the nanowalls by drop-by-drop ex situ FE-SEM analysis provides insight into possible structure formation mechanisms. Further investigation addresses the thermal stability of the particle morphology and the enhancement of the surface-to-volume ratio by heat treatment (examined by N2 physisorption).}}, author = {{Engelkemeier, Katja and Lindner, Jörg and Bürger, Julius and Vaupel, Kathrin and Hartmann, Marc and Tiemann, Michael and Hoyer, Kay-Peter and Schaper, Mirko}}, issn = {{0957-4484}}, journal = {{Nanotechnology}}, pages = {{095701}}, title = {{{Nano-architectural complexity of zinc oxide nanowall hollow microspheres and their structural properties}}}, doi = {{10.1088/1361-6528/ab55bc}}, volume = {{31}}, year = {{2020}}, } @article{41520, author = {{Wu, Haoran and Bill, T. and Teng, Z.J. and Pramanik, Sudipta and Hoyer, Kay-Peter and Schaper, Mirko and Starke, Peter}}, issn = {{0921-5093}}, journal = {{Materials Science and Engineering: A}}, keywords = {{Mechanical Engineering, Mechanics of Materials, Condensed Matter Physics, General Materials Science}}, publisher = {{Elsevier BV}}, title = {{{Characterization of the fatigue behaviour for SAE 1045 steel without and with load-free sequences based on non-destructive, X-ray diffraction and transmission electron microscopic investigations}}}, doi = {{10.1016/j.msea.2020.139597}}, volume = {{794}}, year = {{2020}}, } @article{41521, author = {{Tillmann, Wolfgang and Lopes Dias, Nelson Filipe and Stangier, Dominic and Hagen, Leif and Schaper, Mirko and Hengsbach, Florian and Hoyer, Kay-Peter}}, issn = {{0257-8972}}, journal = {{Surface and Coatings Technology}}, keywords = {{Materials Chemistry, Surfaces, Coatings and Films, Surfaces and Interfaces, Condensed Matter Physics, General Chemistry}}, publisher = {{Elsevier BV}}, title = {{{Tribo-mechanical properties and adhesion behavior of DLC coatings sputtered onto 36NiCrMo16 produced by selective laser melting}}}, doi = {{10.1016/j.surfcoat.2020.125748}}, volume = {{394}}, year = {{2020}}, } @article{41522, author = {{Andreiev, Anatolii and Hoyer, Kay-Peter and Grydin, Olexandr and Frolov, Yaroslav and Schaper, Mirko}}, issn = {{0933-5137}}, journal = {{Materialwissenschaft und Werkstofftechnik}}, keywords = {{Mechanical Engineering, Mechanics of Materials, Condensed Matter Physics, General Materials Science}}, number = {{4}}, pages = {{517--530}}, publisher = {{Wiley}}, title = {{{Degradable silver‐based alloys}}}, doi = {{10.1002/mawe.201900191}}, volume = {{51}}, year = {{2020}}, } @article{24254, author = {{Tillmann, Wolfgang and Hagen, Leif and Garthe, Kai-Uwe and Hoyer, Kay-Peter and Schaper, Mirko}}, issn = {{0933-5137}}, journal = {{Materialwissenschaft und Werkstofftechnik}}, pages = {{1452--1464}}, title = {{{Effect of substrate pre‐treatment on the low cycle fatigue performance of tungsten carbide‐cobalt coated additive manufactured 316 L substrates}}}, doi = {{10.1002/mawe.202000109}}, year = {{2020}}, } @article{24092, abstract = {{AbstractDifferent studies have been demonstrated that the surface integrity of substrate bulk materials to be coated has a significant impact on the adhesion of thermally sprayed coatings. It is known that the surface integrity of parts processed by selective laser melting (SLM) differs from those obtained from bulk materials. Although 316L stainless steel is among the most investigated material for SLM, the adhesion of thermally sprayed coatings on 316L stainless steel substrates processed by SLM has not been studied yet. This study aims at evaluating the effect of various mechanical pre-treatments onto 316L stainless steel substrates processed by SLM and their effect on the adhesion of high velocity oxy-fuel (HVOF)-sprayed WC-Co coatings. To differentiate between topographical effects and residual stress-related phenomena, a stress-relief heat treatment of the SLM substrates served as a reference throughout the investigations. The differently pre-treated SLM substrates were investigated with regard to the surface roughness and residual stresses. For the HVOF-sprayed SLM composites, Vickers interfacial indentation tests were conducted to assess the resulting coating adhesion. The findings demonstrated that the HVOF-sprayed WC-Co coatings predominantly exhibit good adhesion to the SLM 316L substrates. However, it was found that the stress state in the SLM 316L substrate surface is more likely to affect the adhesion of the WC-Co coating, while the substrate surface roughness showed a marginal effect.}}, author = {{Tillmann, Wolfgang and Hagen, Leif and Schaak, Christopher and Liß, Jan and Schaper, Mirko and Hoyer, Kay-Peter and Aydinöz, Mehmet Esat and Garthe, Kai-Uwe}}, issn = {{1059-9630}}, journal = {{Journal of Thermal Spray Technology}}, pages = {{1396--1409}}, title = {{{Adhesion of HVOF-Sprayed WC-Co Coatings on 316L Substrates Processed by SLM}}}, doi = {{10.1007/s11666-020-01081-y}}, year = {{2020}}, } @article{24255, abstract = {{AbstractDifferent studies have been demonstrated that the surface integrity of substrate bulk materials to be coated has a significant impact on the adhesion of thermally sprayed coatings. It is known that the surface integrity of parts processed by selective laser melting (SLM) differs from those obtained from bulk materials. Although 316L stainless steel is among the most investigated material for SLM, the adhesion of thermally sprayed coatings on 316L stainless steel substrates processed by SLM has not been studied yet. This study aims at evaluating the effect of various mechanical pre-treatments onto 316L stainless steel substrates processed by SLM and their effect on the adhesion of high velocity oxy-fuel (HVOF)-sprayed WC-Co coatings. To differentiate between topographical effects and residual stress-related phenomena, a stress-relief heat treatment of the SLM substrates served as a reference throughout the investigations. The differently pre-treated SLM substrates were investigated with regard to the surface roughness and residual stresses. For the HVOF-sprayed SLM composites, Vickers interfacial indentation tests were conducted to assess the resulting coating adhesion. The findings demonstrated that the HVOF-sprayed WC-Co coatings predominantly exhibit good adhesion to the SLM 316L substrates. However, it was found that the stress state in the SLM 316L substrate surface is more likely to affect the adhesion of the WC-Co coating, while the substrate surface roughness showed a marginal effect.}}, author = {{Tillmann, W. and Hagen, L. and Schaak, C. and Liß, J. and Schaper, Mirko and Hoyer, Kay-Peter and Aydinöz, M. E. and Garthe, Kai-Uwe}}, issn = {{1059-9630}}, journal = {{Journal of Thermal Spray Technology}}, pages = {{1396--1409}}, title = {{{Adhesion of HVOF-Sprayed WC-Co Coatings on 316L Substrates Processed by SLM}}}, doi = {{10.1007/s11666-020-01081-y}}, year = {{2020}}, } @article{24093, author = {{Wu, Haoran and Bill, Tobias and Teng, Zhenjie and Pramanik, Sudipta and Hoyer, Kay-Peter and Schaper, Mirko and Starke, Peter}}, issn = {{0921-5093}}, journal = {{Materials Science and Engineering: A}}, title = {{{Characterization of the fatigue behaviour for SAE 1045 steel without and with load-free sequences based on non-destructive, X-ray diffraction and transmission electron microscopic investigations}}}, doi = {{10.1016/j.msea.2020.139597}}, year = {{2020}}, } @article{24094, author = {{Tillmann, Wolfgang and Lopes Dias, Nelson Filipe and Stangier, Dominic and Hagen, Leif and Schaper, Mirko and Hengsbach, Florian and Hoyer, Kay-Peter}}, issn = {{0257-8972}}, journal = {{Surface and Coatings Technology}}, title = {{{Tribo-mechanical properties and adhesion behavior of DLC coatings sputtered onto 36NiCrMo16 produced by selective laser melting}}}, doi = {{10.1016/j.surfcoat.2020.125748}}, year = {{2020}}, } @article{24091, author = {{Tillmann, Wolfgang and Hagen, Leif and Garthe, Kai-Uwe and Hoyer, Kay-Peter and Schaper, Mirko}}, issn = {{0933-5137}}, journal = {{Materialwissenschaft und Werkstofftechnik}}, pages = {{1452--1464}}, title = {{{Effect of substrate pre‐treatment on the low cycle fatigue performance of tungsten carbide‐cobalt coated additive manufactured 316 L substrates}}}, doi = {{10.1002/mawe.202000109}}, year = {{2020}}, }