[{"publication":"Chemistry of Materials","extern":"1","abstract":[{"lang":"eng","text":"Periodically ordered mesoporous magnesium oxide was synthesized in a double replication procedure. Mesoporous SBA-15 silica and CMK-3 carbon were successively used as hard structure matrixes. The carbon pore system was infiltrated with Mg(NO3)2, which was then converted to MgO at 573 K; the carbon matrix was finally removed by thermal combustion. The structure of the mesoporous MgO corresponds to that of the original SBA-15 silica. The products consist of hexagonally arranged cylindrical mesopores and crystalline pore walls. The efficiency of the replication series was studied by variation of the infiltration method and comprehensive pore size analysis of all involved mesoporous materials. The in situ formation of MgO inside the CMK-3 carbon pore system was monitored by thermal analysis. Postsynthetic treatment of the products at 823 K in a vacuum prior to removal of the carbon matrix was found to improve the crystallinity but to diminish the periodic order of the pore system."}],"date_created":"2021-10-09T09:45:04Z","type":"journal_article","department":[{"_id":"35"},{"_id":"2"},{"_id":"307"}],"title":"Synthesis of Mesoporous Magnesium Oxide by CMK-3 Carbon Structure Replication","year":"2006","publication_identifier":{"issn":["0897-4756","1520-5002"]},"author":[{"first_name":"Jan","last_name":"Roggenbuck","full_name":"Roggenbuck, Jan"},{"first_name":"Günter","last_name":"Koch","full_name":"Koch, Günter"},{"orcid":"0000-0003-1711-2722","last_name":"Tiemann","first_name":"Michael","full_name":"Tiemann, Michael","id":"23547"}],"publication_status":"published","date_updated":"2023-03-09T08:58:00Z","article_type":"original","language":[{"iso":"eng"}],"doi":"10.1021/cm060740s","citation":{"ieee":"J. Roggenbuck, G. Koch, and M. Tiemann, “Synthesis of Mesoporous Magnesium Oxide by CMK-3 Carbon Structure Replication,” Chemistry of Materials, pp. 4151–4156, 2006, doi: 10.1021/cm060740s.","apa":"Roggenbuck, J., Koch, G., & Tiemann, M. (2006). Synthesis of Mesoporous Magnesium Oxide by CMK-3 Carbon Structure Replication. Chemistry of Materials, 4151–4156. https://doi.org/10.1021/cm060740s","short":"J. Roggenbuck, G. Koch, M. Tiemann, Chemistry of Materials (2006) 4151–4156.","chicago":"Roggenbuck, Jan, Günter Koch, and Michael Tiemann. “Synthesis of Mesoporous Magnesium Oxide by CMK-3 Carbon Structure Replication.” Chemistry of Materials, 2006, 4151–56. https://doi.org/10.1021/cm060740s.","mla":"Roggenbuck, Jan, et al. “Synthesis of Mesoporous Magnesium Oxide by CMK-3 Carbon Structure Replication.” Chemistry of Materials, 2006, pp. 4151–56, doi:10.1021/cm060740s.","bibtex":"@article{Roggenbuck_Koch_Tiemann_2006, title={Synthesis of Mesoporous Magnesium Oxide by CMK-3 Carbon Structure Replication}, DOI={10.1021/cm060740s}, journal={Chemistry of Materials}, author={Roggenbuck, Jan and Koch, Günter and Tiemann, Michael}, year={2006}, pages={4151–4156} }","ama":"Roggenbuck J, Koch G, Tiemann M. Synthesis of Mesoporous Magnesium Oxide by CMK-3 Carbon Structure Replication. Chemistry of Materials. Published online 2006:4151-4156. doi:10.1021/cm060740s"},"quality_controlled":"1","status":"public","page":"4151-4156","_id":"25991","user_id":"23547"},{"volume":38,"user_id":"466","publisher":"American Chemical Society (ACS)","_id":"35355","page":"9772-9782","status":"public","quality_controlled":"1","citation":{"mla":"Kleinschmidt, Felix, et al. “Lamellar Liquid Single Crystal Hydrogels:  Synthesis and Investigation of Anisotropic Water Diffusion and Swelling.” Macromolecules, vol. 38, no. 23, American Chemical Society (ACS), 2005, pp. 9772–82, doi:10.1021/ma051479o.","bibtex":"@article{Kleinschmidt_Hickl_Saalwächter_Schmidt_Finkelmann_2005, title={Lamellar Liquid Single Crystal Hydrogels:  Synthesis and Investigation of Anisotropic Water Diffusion and Swelling}, volume={38}, DOI={10.1021/ma051479o}, number={23}, journal={Macromolecules}, publisher={American Chemical Society (ACS)}, author={Kleinschmidt, Felix and Hickl, Markus and Saalwächter, Kay and Schmidt, Claudia and Finkelmann, Heino}, year={2005}, pages={9772–9782} }","ama":"Kleinschmidt F, Hickl M, Saalwächter K, Schmidt C, Finkelmann H. Lamellar Liquid Single Crystal Hydrogels:  Synthesis and Investigation of Anisotropic Water Diffusion and Swelling. Macromolecules. 2005;38(23):9772-9782. doi:10.1021/ma051479o","ieee":"F. Kleinschmidt, M. Hickl, K. Saalwächter, C. Schmidt, and H. Finkelmann, “Lamellar Liquid Single Crystal Hydrogels:  Synthesis and Investigation of Anisotropic Water Diffusion and Swelling,” Macromolecules, vol. 38, no. 23, pp. 9772–9782, 2005, doi: 10.1021/ma051479o.","apa":"Kleinschmidt, F., Hickl, M., Saalwächter, K., Schmidt, C., & Finkelmann, H. (2005). Lamellar Liquid Single Crystal Hydrogels:  Synthesis and Investigation of Anisotropic Water Diffusion and Swelling. Macromolecules, 38(23), 9772–9782. https://doi.org/10.1021/ma051479o","chicago":"Kleinschmidt, Felix, Markus Hickl, Kay Saalwächter, Claudia Schmidt, and Heino Finkelmann. “Lamellar Liquid Single Crystal Hydrogels:  Synthesis and Investigation of Anisotropic Water Diffusion and Swelling.” Macromolecules 38, no. 23 (2005): 9772–82. https://doi.org/10.1021/ma051479o.","short":"F. Kleinschmidt, M. Hickl, K. Saalwächter, C. Schmidt, H. Finkelmann, Macromolecules 38 (2005) 9772–9782."},"doi":"10.1021/ma051479o","language":[{"iso":"eng"}],"intvolume":" 38","article_type":"original","date_updated":"2023-01-07T11:24:34Z","publication_status":"published","author":[{"last_name":"Kleinschmidt","first_name":"Felix","full_name":"Kleinschmidt, Felix"},{"full_name":"Hickl, Markus","last_name":"Hickl","first_name":"Markus"},{"full_name":"Saalwächter, Kay","first_name":"Kay","last_name":"Saalwächter"},{"first_name":"Claudia","last_name":"Schmidt","orcid":"0000-0003-3179-9997","full_name":"Schmidt, Claudia","id":"466"},{"full_name":"Finkelmann, Heino","last_name":"Finkelmann","first_name":"Heino"}],"publication_identifier":{"issn":["0024-9297","1520-5835"]},"title":"Lamellar Liquid Single Crystal Hydrogels:  Synthesis and Investigation of Anisotropic Water Diffusion and Swelling","year":"2005","department":[{"_id":"2"},{"_id":"315"}],"keyword":["Materials Chemistry","Inorganic Chemistry","Polymers and Plastics","Organic Chemistry"],"type":"journal_article","date_created":"2023-01-06T13:14:06Z","publication":"Macromolecules","issue":"23"},{"author":[{"full_name":"Becker, Patrick","first_name":"Patrick","last_name":"Becker"},{"last_name":"Siebert","first_name":"Hartmut","full_name":"Siebert, Hartmut"},{"first_name":"Laurence","last_name":"Noirez","full_name":"Noirez, Laurence"},{"full_name":"Schmidt, Claudia","orcid":"0000-0003-3179-9997","first_name":"Claudia","last_name":"Schmidt","id":"466"}],"publication_identifier":{"issn":["1022-1360","1521-3900"]},"title":"Shear-Induced Order in Nematic Polymers","year":"2005","article_type":"original","intvolume":" 220","publication_status":"published","date_updated":"2023-01-07T11:24:02Z","language":[{"iso":"eng"}],"doi":"10.1002/masy.200550209","publication":"Macromolecular Symposia","issue":"1","date_created":"2023-01-06T13:14:25Z","department":[{"_id":"2"},{"_id":"315"}],"keyword":["Materials Chemistry","Polymers and Plastics","Organic Chemistry","Condensed Matter Physics"],"type":"journal_article","status":"public","_id":"35356","publisher":"Wiley","page":"111-122","volume":220,"user_id":"466","citation":{"apa":"Becker, P., Siebert, H., Noirez, L., & Schmidt, C. (2005). Shear-Induced Order in Nematic Polymers. Macromolecular Symposia, 220(1), 111–122. https://doi.org/10.1002/masy.200550209","ieee":"P. Becker, H. Siebert, L. Noirez, and C. Schmidt, “Shear-Induced Order in Nematic Polymers,” Macromolecular Symposia, vol. 220, no. 1, pp. 111–122, 2005, doi: 10.1002/masy.200550209.","short":"P. Becker, H. Siebert, L. Noirez, C. Schmidt, Macromolecular Symposia 220 (2005) 111–122.","chicago":"Becker, Patrick, Hartmut Siebert, Laurence Noirez, and Claudia Schmidt. “Shear-Induced Order in Nematic Polymers.” Macromolecular Symposia 220, no. 1 (2005): 111–22. https://doi.org/10.1002/masy.200550209.","mla":"Becker, Patrick, et al. “Shear-Induced Order in Nematic Polymers.” Macromolecular Symposia, vol. 220, no. 1, Wiley, 2005, pp. 111–22, doi:10.1002/masy.200550209.","ama":"Becker P, Siebert H, Noirez L, Schmidt C. Shear-Induced Order in Nematic Polymers. Macromolecular Symposia. 2005;220(1):111-122. doi:10.1002/masy.200550209","bibtex":"@article{Becker_Siebert_Noirez_Schmidt_2005, title={Shear-Induced Order in Nematic Polymers}, volume={220}, DOI={10.1002/masy.200550209}, number={1}, journal={Macromolecular Symposia}, publisher={Wiley}, author={Becker, Patrick and Siebert, Hartmut and Noirez, Laurence and Schmidt, Claudia}, year={2005}, pages={111–122} }"}},{"date_created":"2023-01-24T19:10:38Z","department":[{"_id":"313"},{"_id":"638"}],"type":"journal_article","keyword":["Physics and Astronomy (miscellaneous)"],"publication":"Applied Physics Letters","issue":"24","language":[{"iso":"eng"}],"article_number":"241105","doi":"10.1063/1.2142100","author":[{"first_name":"Heinrich","last_name":"Matthias","full_name":"Matthias, Heinrich"},{"full_name":"Röder, Thorsten","first_name":"Thorsten","last_name":"Röder"},{"last_name":"Wehrspohn","first_name":"Ralf B.","full_name":"Wehrspohn, Ralf B."},{"id":"254","full_name":"Kitzerow, Heinz-Siegfried","last_name":"Kitzerow","first_name":"Heinz-Siegfried"},{"full_name":"Matthias, Sven","first_name":"Sven","last_name":"Matthias"},{"full_name":"Picken, Stephen J.","first_name":"Stephen J.","last_name":"Picken"}],"publication_identifier":{"issn":["0003-6951","1077-3118"]},"year":"2005","title":"Spatially periodic liquid crystal director field appearing in a photonic crystal template","intvolume":" 87","date_updated":"2023-01-24T19:11:03Z","publication_status":"published","citation":{"chicago":"Matthias, Heinrich, Thorsten Röder, Ralf B. Wehrspohn, Heinz-Siegfried Kitzerow, Sven Matthias, and Stephen J. Picken. “Spatially Periodic Liquid Crystal Director Field Appearing in a Photonic Crystal Template.” Applied Physics Letters 87, no. 24 (2005). https://doi.org/10.1063/1.2142100.","short":"H. Matthias, T. Röder, R.B. Wehrspohn, H.-S. Kitzerow, S. Matthias, S.J. Picken, Applied Physics Letters 87 (2005).","ieee":"H. Matthias, T. Röder, R. B. Wehrspohn, H.-S. Kitzerow, S. Matthias, and S. J. Picken, “Spatially periodic liquid crystal director field appearing in a photonic crystal template,” Applied Physics Letters, vol. 87, no. 24, Art. no. 241105, 2005, doi: 10.1063/1.2142100.","apa":"Matthias, H., Röder, T., Wehrspohn, R. B., Kitzerow, H.-S., Matthias, S., & Picken, S. J. (2005). Spatially periodic liquid crystal director field appearing in a photonic crystal template. Applied Physics Letters, 87(24), Article 241105. https://doi.org/10.1063/1.2142100","bibtex":"@article{Matthias_Röder_Wehrspohn_Kitzerow_Matthias_Picken_2005, title={Spatially periodic liquid crystal director field appearing in a photonic crystal template}, volume={87}, DOI={10.1063/1.2142100}, number={24241105}, journal={Applied Physics Letters}, publisher={AIP Publishing}, author={Matthias, Heinrich and Röder, Thorsten and Wehrspohn, Ralf B. and Kitzerow, Heinz-Siegfried and Matthias, Sven and Picken, Stephen J.}, year={2005} }","ama":"Matthias H, Röder T, Wehrspohn RB, Kitzerow H-S, Matthias S, Picken SJ. Spatially periodic liquid crystal director field appearing in a photonic crystal template. Applied Physics Letters. 2005;87(24). doi:10.1063/1.2142100","mla":"Matthias, Heinrich, et al. “Spatially Periodic Liquid Crystal Director Field Appearing in a Photonic Crystal Template.” Applied Physics Letters, vol. 87, no. 24, 241105, AIP Publishing, 2005, doi:10.1063/1.2142100."},"_id":"39764","publisher":"AIP Publishing","volume":87,"user_id":"254","status":"public"},{"citation":{"short":"G. Mertens, R.B. Wehrspohn, H.-S. Kitzerow, S. Matthias, C. Jamois, U. Gösele, Applied Physics Letters 87 (2005).","chicago":"Mertens, G., R. B. Wehrspohn, Heinz-Siegfried Kitzerow, S. Matthias, C. Jamois, and U. Gösele. “Tunable Defect Mode in a Three-Dimensional Photonic Crystal.” Applied Physics Letters 87, no. 24 (2005). https://doi.org/10.1063/1.2139846.","apa":"Mertens, G., Wehrspohn, R. B., Kitzerow, H.-S., Matthias, S., Jamois, C., & Gösele, U. (2005). Tunable defect mode in a three-dimensional photonic crystal. Applied Physics Letters, 87(24), Article 241108. https://doi.org/10.1063/1.2139846","ieee":"G. Mertens, R. B. Wehrspohn, H.-S. Kitzerow, S. Matthias, C. Jamois, and U. Gösele, “Tunable defect mode in a three-dimensional photonic crystal,” Applied Physics Letters, vol. 87, no. 24, Art. no. 241108, 2005, doi: 10.1063/1.2139846.","ama":"Mertens G, Wehrspohn RB, Kitzerow H-S, Matthias S, Jamois C, Gösele U. Tunable defect mode in a three-dimensional photonic crystal. Applied Physics Letters. 2005;87(24). doi:10.1063/1.2139846","bibtex":"@article{Mertens_Wehrspohn_Kitzerow_Matthias_Jamois_Gösele_2005, title={Tunable defect mode in a three-dimensional photonic crystal}, volume={87}, DOI={10.1063/1.2139846}, number={24241108}, journal={Applied Physics Letters}, publisher={AIP Publishing}, author={Mertens, G. and Wehrspohn, R. B. and Kitzerow, Heinz-Siegfried and Matthias, S. and Jamois, C. and Gösele, U.}, year={2005} }","mla":"Mertens, G., et al. “Tunable Defect Mode in a Three-Dimensional Photonic Crystal.” Applied Physics Letters, vol. 87, no. 24, 241108, AIP Publishing, 2005, doi:10.1063/1.2139846."},"status":"public","volume":87,"user_id":"254","_id":"39767","publisher":"AIP Publishing","issue":"24","publication":"Applied Physics Letters","department":[{"_id":"313"},{"_id":"638"}],"keyword":["Physics and Astronomy (miscellaneous)"],"type":"journal_article","date_created":"2023-01-24T19:12:37Z","intvolume":" 87","publication_status":"published","date_updated":"2023-01-24T19:13:14Z","author":[{"last_name":"Mertens","first_name":"G.","full_name":"Mertens, G."},{"last_name":"Wehrspohn","first_name":"R. B.","full_name":"Wehrspohn, R. B."},{"id":"254","full_name":"Kitzerow, Heinz-Siegfried","first_name":"Heinz-Siegfried","last_name":"Kitzerow"},{"last_name":"Matthias","first_name":"S.","full_name":"Matthias, S."},{"full_name":"Jamois, C.","last_name":"Jamois","first_name":"C."},{"last_name":"Gösele","first_name":"U.","full_name":"Gösele, U."}],"publication_identifier":{"issn":["0003-6951","1077-3118"]},"year":"2005","title":"Tunable defect mode in a three-dimensional photonic crystal","doi":"10.1063/1.2139846","language":[{"iso":"eng"}],"article_number":"241108"},{"issue":"3","publication":"Applied Physics Letters","keyword":["Physics and Astronomy (miscellaneous)"],"type":"journal_article","department":[{"_id":"313"},{"_id":"638"}],"date_created":"2023-01-24T19:13:33Z","publication_status":"published","date_updated":"2023-01-24T19:13:50Z","intvolume":" 86","title":"Photorefractive polymer-dispersed liquid crystal based on a photoconducting polysiloxane","year":"2005","author":[{"full_name":"Paelke, Lutz","first_name":"Lutz","last_name":"Paelke"},{"last_name":"Kitzerow","first_name":"Heinz-Siegfried","full_name":"Kitzerow, Heinz-Siegfried","id":"254"},{"full_name":"Strohriegl, Peter","first_name":"Peter","last_name":"Strohriegl"}],"publication_identifier":{"issn":["0003-6951","1077-3118"]},"doi":"10.1063/1.1852082","article_number":"031104","language":[{"iso":"eng"}],"citation":{"apa":"Paelke, L., Kitzerow, H.-S., & Strohriegl, P. (2005). Photorefractive polymer-dispersed liquid crystal based on a photoconducting polysiloxane. Applied Physics Letters, 86(3), Article 031104. https://doi.org/10.1063/1.1852082","ieee":"L. Paelke, H.-S. Kitzerow, and P. Strohriegl, “Photorefractive polymer-dispersed liquid crystal based on a photoconducting polysiloxane,” Applied Physics Letters, vol. 86, no. 3, Art. no. 031104, 2005, doi: 10.1063/1.1852082.","short":"L. Paelke, H.-S. Kitzerow, P. Strohriegl, Applied Physics Letters 86 (2005).","chicago":"Paelke, Lutz, Heinz-Siegfried Kitzerow, and Peter Strohriegl. “Photorefractive Polymer-Dispersed Liquid Crystal Based on a Photoconducting Polysiloxane.” Applied Physics Letters 86, no. 3 (2005). https://doi.org/10.1063/1.1852082.","mla":"Paelke, Lutz, et al. “Photorefractive Polymer-Dispersed Liquid Crystal Based on a Photoconducting Polysiloxane.” Applied Physics Letters, vol. 86, no. 3, 031104, AIP Publishing, 2005, doi:10.1063/1.1852082.","ama":"Paelke L, Kitzerow H-S, Strohriegl P. Photorefractive polymer-dispersed liquid crystal based on a photoconducting polysiloxane. Applied Physics Letters. 2005;86(3). doi:10.1063/1.1852082","bibtex":"@article{Paelke_Kitzerow_Strohriegl_2005, title={Photorefractive polymer-dispersed liquid crystal based on a photoconducting polysiloxane}, volume={86}, DOI={10.1063/1.1852082}, number={3031104}, journal={Applied Physics Letters}, publisher={AIP Publishing}, author={Paelke, Lutz and Kitzerow, Heinz-Siegfried and Strohriegl, Peter}, year={2005} }"},"status":"public","user_id":"254","volume":86,"_id":"39768","publisher":"AIP Publishing"},{"citation":{"chicago":"Stich, N., and Heinz-Siegfried Kitzerow. “Superposition of Patterns in Cross-Linked Liquid Crystals.” Journal of Applied Physics 97, no. 3 (2005). https://doi.org/10.1063/1.1832744.","short":"N. Stich, H.-S. Kitzerow, Journal of Applied Physics 97 (2005).","ieee":"N. Stich and H.-S. Kitzerow, “Superposition of patterns in cross-linked liquid crystals,” Journal of Applied Physics, vol. 97, no. 3, Art. no. 033519, 2005, doi: 10.1063/1.1832744.","apa":"Stich, N., & Kitzerow, H.-S. (2005). Superposition of patterns in cross-linked liquid crystals. Journal of Applied Physics, 97(3), Article 033519. https://doi.org/10.1063/1.1832744","bibtex":"@article{Stich_Kitzerow_2005, title={Superposition of patterns in cross-linked liquid crystals}, volume={97}, DOI={10.1063/1.1832744}, number={3033519}, journal={Journal of Applied Physics}, publisher={AIP Publishing}, author={Stich, N. and Kitzerow, Heinz-Siegfried}, year={2005} }","ama":"Stich N, Kitzerow H-S. Superposition of patterns in cross-linked liquid crystals. Journal of Applied Physics. 2005;97(3). doi:10.1063/1.1832744","mla":"Stich, N., and Heinz-Siegfried Kitzerow. “Superposition of Patterns in Cross-Linked Liquid Crystals.” Journal of Applied Physics, vol. 97, no. 3, 033519, AIP Publishing, 2005, doi:10.1063/1.1832744."},"_id":"39770","publisher":"AIP Publishing","user_id":"254","volume":97,"status":"public","date_created":"2023-01-24T19:14:46Z","type":"journal_article","keyword":["General Physics and Astronomy"],"department":[{"_id":"313"},{"_id":"638"}],"publication":"Journal of Applied Physics","issue":"3","article_number":"033519","language":[{"iso":"eng"}],"doi":"10.1063/1.1832744","year":"2005","title":"Superposition of patterns in cross-linked liquid crystals","publication_identifier":{"issn":["0021-8979","1089-7550"]},"author":[{"first_name":"N.","last_name":"Stich","full_name":"Stich, N."},{"full_name":"Kitzerow, Heinz-Siegfried","first_name":"Heinz-Siegfried","last_name":"Kitzerow","id":"254"}],"publication_status":"published","date_updated":"2023-01-24T19:15:41Z","intvolume":" 97"},{"volume":2,"user_id":"254","publisher":"Wiley","_id":"39973","page":"628-632","status":"public","citation":{"chicago":"Kitzerow, Heinz-Siegfried. “News about Soft Condensed Matter—A Liquid Crystal Meeting Review.” ChemPhysChem 2, no. 10 (2005): 628–32. https://doi.org/10.1002/1439-7641(20011015)2:10<628::aid-cphc628>3.0.co;2-7.","short":"H.-S. Kitzerow, ChemPhysChem 2 (2005) 628–632.","apa":"Kitzerow, H.-S. (2005). News about Soft Condensed Matter—A Liquid Crystal Meeting Review. ChemPhysChem, 2(10), 628–632. https://doi.org/10.1002/1439-7641(20011015)2:10<628::aid-cphc628>3.0.co;2-7","ieee":"H.-S. Kitzerow, “News about Soft Condensed Matter—A Liquid Crystal Meeting Review,” ChemPhysChem, vol. 2, no. 10, pp. 628–632, 2005, doi: 10.1002/1439-7641(20011015)2:10<628::aid-cphc628>3.0.co;2-7.","ama":"Kitzerow H-S. News about Soft Condensed Matter—A Liquid Crystal Meeting Review. 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Published online 2005:2113-2119. doi:10.1002/cphc.200500163","chicago":"Tiemann, Michael, Özlem Weiß, Juha Hartikainen, Frank Marlow, and Mika Lindén. “Early Stages of ZnS Nanoparticle Growth Studied by In-Situ Stopped-Flow UV Absorption Spectroscopy.” ChemPhysChem, 2005, 2113–19. https://doi.org/10.1002/cphc.200500163.","bibtex":"@article{Tiemann_Weiß_Hartikainen_Marlow_Lindén_2005, title={Early Stages of ZnS Nanoparticle Growth Studied by In-Situ Stopped-Flow UV Absorption Spectroscopy}, DOI={10.1002/cphc.200500163}, journal={ChemPhysChem}, author={Tiemann, Michael and Weiß, Özlem and Hartikainen, Juha and Marlow, Frank and Lindén, Mika}, year={2005}, pages={2113–2119} }"},"quality_controlled":"1","year":"2005","title":"Early Stages of ZnS Nanoparticle Growth Studied by In-Situ Stopped-Flow UV Absorption Spectroscopy","publication_identifier":{"issn":["1439-4235","1439-7641"]},"author":[{"last_name":"Tiemann","first_name":"Michael","orcid":"0000-0003-1711-2722","full_name":"Tiemann, Michael","id":"23547"},{"full_name":"Weiß, Özlem","last_name":"Weiß","first_name":"Özlem"},{"full_name":"Hartikainen, Juha","first_name":"Juha","last_name":"Hartikainen"},{"full_name":"Marlow, Frank","first_name":"Frank","last_name":"Marlow"},{"full_name":"Lindén, Mika","first_name":"Mika","last_name":"Lindén"}],"date_updated":"2023-03-09T08:58:26Z","publication_status":"published","article_type":"original","language":[{"iso":"eng"}],"doi":"10.1002/cphc.200500163","publication":"ChemPhysChem","abstract":[{"lang":"eng","text":"The early stages of ZnS nanoparticle growth from supersaturated solution are investigated in situ by stopped-flow UV absorption spectroscopy with a time resolution of 1.28 ms. A model for data analysis is suggested which makes it possible to study both the average particle radius and the concentration. The average radii lie in the sub-nanometer range. During the first 40 ms, growth is predominantly governed by ripening."}],"extern":"1","date_created":"2021-10-09T09:48:34Z","type":"journal_article","department":[{"_id":"35"},{"_id":"2"},{"_id":"307"}]},{"doi":"10.1021/ja043605u","language":[{"iso":"eng"}],"article_type":"original","date_updated":"2023-03-09T08:58:46Z","publication_status":"published","publication_identifier":{"issn":["0002-7863","1520-5126"]},"author":[{"full_name":"Roggenbuck, Jan","first_name":"Jan","last_name":"Roggenbuck"},{"id":"23547","first_name":"Michael","last_name":"Tiemann","orcid":"0000-0003-1711-2722","full_name":"Tiemann, Michael"}],"year":"2005","title":"Ordered Mesoporous Magnesium Oxide with High Thermal Stability Synthesized by Exotemplating Using CMK-3 Carbon","department":[{"_id":"35"},{"_id":"2"},{"_id":"307"}],"type":"journal_article","date_created":"2021-10-09T09:47:51Z","abstract":[{"text":"Periodically ordered mesoporous magnesium oxides were synthesized by utilization of mesoporous CMK-3 carbon as exotemplate. The products exhibit high thermal stability and basic properties, which makes them promising for application in heterogeneous basic catalysis.","lang":"eng"}],"extern":"1","publication":"Journal of the American Chemical Society","user_id":"23547","_id":"25994","page":"1096-1097","status":"public","quality_controlled":"1","citation":{"apa":"Roggenbuck, J., & Tiemann, M. (2005). Ordered Mesoporous Magnesium Oxide with High Thermal Stability Synthesized by Exotemplating Using CMK-3 Carbon. Journal of the American Chemical Society, 1096–1097. https://doi.org/10.1021/ja043605u","mla":"Roggenbuck, Jan, and Michael Tiemann. “Ordered Mesoporous Magnesium Oxide with High Thermal Stability Synthesized by Exotemplating Using CMK-3 Carbon.” Journal of the American Chemical Society, 2005, pp. 1096–97, doi:10.1021/ja043605u.","ieee":"J. Roggenbuck and M. Tiemann, “Ordered Mesoporous Magnesium Oxide with High Thermal Stability Synthesized by Exotemplating Using CMK-3 Carbon,” Journal of the American Chemical Society, pp. 1096–1097, 2005, doi: 10.1021/ja043605u.","chicago":"Roggenbuck, Jan, and Michael Tiemann. “Ordered Mesoporous Magnesium Oxide with High Thermal Stability Synthesized by Exotemplating Using CMK-3 Carbon.” Journal of the American Chemical Society, 2005, 1096–97. https://doi.org/10.1021/ja043605u.","ama":"Roggenbuck J, Tiemann M. Ordered Mesoporous Magnesium Oxide with High Thermal Stability Synthesized by Exotemplating Using CMK-3 Carbon. Journal of the American Chemical Society. Published online 2005:1096-1097. doi:10.1021/ja043605u","short":"J. Roggenbuck, M. Tiemann, Journal of the American Chemical Society (2005) 1096–1097.","bibtex":"@article{Roggenbuck_Tiemann_2005, title={Ordered Mesoporous Magnesium Oxide with High Thermal Stability Synthesized by Exotemplating Using CMK-3 Carbon}, DOI={10.1021/ja043605u}, journal={Journal of the American Chemical Society}, author={Roggenbuck, Jan and Tiemann, Michael}, year={2005}, pages={1096–1097} }"}},{"citation":{"mla":"Herres‐Pawlis, Sonja, et al. “A Library of Peralkylated Bis‐guanidine Ligands for Use in Biomimetic Coordination Chemistry.” European Journal of Organic Chemistry, vol. 2005, no. 22, Wiley, 2005, pp. 4879–90, doi:10.1002/ejoc.200500340.","bibtex":"@article{Herres‐Pawlis_Neuba_Seewald_Seshadri_Egold_Flörke_Henkel_2005, title={A Library of Peralkylated Bis‐guanidine Ligands for Use in Biomimetic Coordination Chemistry}, volume={2005}, DOI={10.1002/ejoc.200500340}, number={22}, journal={European Journal of Organic Chemistry}, publisher={Wiley}, author={Herres‐Pawlis, Sonja and Neuba, Adam and Seewald, Oliver and Seshadri, Tarimala and Egold, Hans and Flörke, Ulrich and Henkel, Gerald}, year={2005}, pages={4879–4890} }","ama":"Herres‐Pawlis S, Neuba A, Seewald O, et al. A Library of Peralkylated Bis‐guanidine Ligands for Use in Biomimetic Coordination Chemistry. European Journal of Organic Chemistry. 2005;2005(22):4879-4890. doi:10.1002/ejoc.200500340","ieee":"S. Herres‐Pawlis et al., “A Library of Peralkylated Bis‐guanidine Ligands for Use in Biomimetic Coordination Chemistry,” European Journal of Organic Chemistry, vol. 2005, no. 22, pp. 4879–4890, 2005, doi: 10.1002/ejoc.200500340.","apa":"Herres‐Pawlis, S., Neuba, A., Seewald, O., Seshadri, T., Egold, H., Flörke, U., & Henkel, G. (2005). A Library of Peralkylated Bis‐guanidine Ligands for Use in Biomimetic Coordination Chemistry. European Journal of Organic Chemistry, 2005(22), 4879–4890. https://doi.org/10.1002/ejoc.200500340","short":"S. Herres‐Pawlis, A. Neuba, O. Seewald, T. Seshadri, H. Egold, U. Flörke, G. Henkel, European Journal of Organic Chemistry 2005 (2005) 4879–4890.","chicago":"Herres‐Pawlis, Sonja, Adam Neuba, Oliver Seewald, Tarimala Seshadri, Hans Egold, Ulrich Flörke, and Gerald Henkel. “A Library of Peralkylated Bis‐guanidine Ligands for Use in Biomimetic Coordination Chemistry.” European Journal of Organic Chemistry 2005, no. 22 (2005): 4879–90. https://doi.org/10.1002/ejoc.200500340."},"volume":2005,"user_id":"495","_id":"58598","publisher":"Wiley","page":"4879-4890","status":"public","department":[{"_id":"321"},{"_id":"35"},{"_id":"301"}],"type":"journal_article","date_created":"2025-02-12T09:27:00Z","abstract":[{"text":"AbstractA series of bis‐guanidine ligands designed for use in biomimetic coordination chemistry has been extended to a library matrix combining unprecedented substitutional flexibility within the guanidyl residues with a wide range of aliphatic and aromatic spacers connecting these functionalities. The underlying protocol can be used with predefined ureas as well as secondary amines to build up these units by reaction with phosgene if the ureas are otherwise unavailable. In the latter case, the resulting urea intermediates do not have to be isolated as the reaction proceeds further with additional phosgene to yield a chloroformamidinium chloride which is transformed into the bis‐guanidine functionality by subsequent reaction with a suitable primary diamine in the presence of triethylamine as an auxiliary base. This concept has been used to synthesise and characterise more then two dozen different bis‐guanidines based on 12 discrete monoguanidine units and seven different spacers. These spacers have been chosen such that the most important phenotypes have been dealt with and which range from rigid to more flexible scaffolds. In addition to spacers with no metal‐binding capabilities, other species containing further donor functions such as N‐methyldiphenyleneamine or pyridine‐2,6‐diyl have also been used. The substitution patterns of the guanidine residues can be classified into acyclic and cyclic types. Among the cyclic types, one subset is characterised by five‐ or six‐membered heterocycles containing both the amino nitrogen atoms and another one by individual N‐heterocyclic systems for each amino nitrogen. Structurally characterised examples are 2‐{2‐[2‐(tetramethylguanidi­no)ethoxy]ethoxy}‐1‐(tetramethylguanidino)ethane (TMG2doo) in its diprotonated form and 2,2′‐bis[2N‐(1,1′,3,3′‐tetramethylguanidine)]diphenyleneamine (TMG2PA) as wellas N1,N3‐bis(dimorpholinomethylene)propane‐1,3‐diamine (DMorphG2p) as free bases. For the permethylated bis‐guanidine derivatives, the barrier to rotation around the (C=N)guanidine bond has been determined by means of temperature‐dependent EXSY 1H NMR spectroscopy to range between 54 and 79 kJ mol–1 depending on the type of spacer. (© Wiley‐VCH Verlag GmbH & Co. KGaA, 69451 Weinheim, Germany, 2005)","lang":"eng"}],"issue":"22","publication":"European Journal of Organic Chemistry","doi":"10.1002/ejoc.200500340","language":[{"iso":"eng"}],"intvolume":" 2005","publication_status":"published","date_updated":"2025-02-12T09:30:43Z","publication_identifier":{"issn":["1434-193X","1099-0690"]},"author":[{"full_name":"Herres‐Pawlis, Sonja","last_name":"Herres‐Pawlis","first_name":"Sonja"},{"full_name":"Neuba, Adam","first_name":"Adam","last_name":"Neuba"},{"full_name":"Seewald, Oliver","first_name":"Oliver","last_name":"Seewald","id":"495"},{"last_name":"Seshadri","first_name":"Tarimala","full_name":"Seshadri, Tarimala"},{"full_name":"Egold, Hans","first_name":"Hans","last_name":"Egold"},{"full_name":"Flörke, Ulrich","last_name":"Flörke","first_name":"Ulrich"},{"last_name":"Henkel","first_name":"Gerald","full_name":"Henkel, Gerald"}],"title":"A Library of Peralkylated Bis‐guanidine Ligands for Use in Biomimetic Coordination Chemistry","year":"2005"},{"_id":"58597","publisher":"Wiley","page":"204-210","volume":632,"user_id":"495","status":"public","citation":{"apa":"Seewald, O., Flörke, U., Egold, H., Haupt, H., & Schwefer, M. (2005). Synthese und Struktur chiraler Heterometallatetrahedrane des Typs [Re2(M1PPh3)(M2PPh3)(μ‐PCy2)(CO)7C≡CPh] (M1 = Ag, Au; M2 = Cu, Ag, Au). Zeitschrift Für Anorganische Und Allgemeine Chemie, 632(2), 204–210. https://doi.org/10.1002/zaac.200500340","ieee":"O. Seewald, U. Flörke, H. Egold, H. Haupt, and M. Schwefer, “Synthese und Struktur chiraler Heterometallatetrahedrane des Typs [Re2(M1PPh3)(M2PPh3)(μ‐PCy2)(CO)7C≡CPh] (M1 = Ag, Au; M2 = Cu, Ag, Au),” Zeitschrift für anorganische und allgemeine Chemie, vol. 632, no. 2, pp. 204–210, 2005, doi: 10.1002/zaac.200500340.","short":"O. Seewald, U. Flörke, H. Egold, H. Haupt, M. Schwefer, Zeitschrift Für Anorganische Und Allgemeine Chemie 632 (2005) 204–210.","chicago":"Seewald, Oliver, Ulrich Flörke, Hans Egold, Hans‐Jürgen Haupt, and Meinhard Schwefer. “Synthese Und Struktur Chiraler Heterometallatetrahedrane Des Typs [Re2(M1PPh3)(M2PPh3)(Μ‐PCy2)(CO)7C≡CPh] (M1 = Ag, Au; M2 = Cu, Ag, Au).” Zeitschrift Für Anorganische Und Allgemeine Chemie 632, no. 2 (2005): 204–10. https://doi.org/10.1002/zaac.200500340.","mla":"Seewald, Oliver, et al. “Synthese Und Struktur Chiraler Heterometallatetrahedrane Des Typs [Re2(M1PPh3)(M2PPh3)(Μ‐PCy2)(CO)7C≡CPh] (M1 = Ag, Au; M2 = Cu, Ag, Au).” Zeitschrift Für Anorganische Und Allgemeine Chemie, vol. 632, no. 2, Wiley, 2005, pp. 204–10, doi:10.1002/zaac.200500340.","ama":"Seewald O, Flörke U, Egold H, Haupt H, Schwefer M. Synthese und Struktur chiraler Heterometallatetrahedrane des Typs [Re2(M1PPh3)(M2PPh3)(μ‐PCy2)(CO)7C≡CPh] (M1 = Ag, Au; M2 = Cu, Ag, Au). Zeitschrift für anorganische und allgemeine Chemie. 2005;632(2):204-210. doi:10.1002/zaac.200500340","bibtex":"@article{Seewald_Flörke_Egold_Haupt_Schwefer_2005, title={Synthese und Struktur chiraler Heterometallatetrahedrane des Typs [Re2(M1PPh3)(M2PPh3)(μ‐PCy2)(CO)7C≡CPh] (M1 = Ag, Au; M2 = Cu, Ag, Au)}, volume={632}, DOI={10.1002/zaac.200500340}, number={2}, journal={Zeitschrift für anorganische und allgemeine Chemie}, publisher={Wiley}, author={Seewald, Oliver and Flörke, Ulrich and Egold, Hans and Haupt, Hans‐Jürgen and Schwefer, Meinhard}, year={2005}, pages={204–210} }"},"language":[{"iso":"eng"}],"doi":"10.1002/zaac.200500340","author":[{"id":"495","full_name":"Seewald, Oliver","first_name":"Oliver","last_name":"Seewald"},{"full_name":"Flörke, Ulrich","first_name":"Ulrich","last_name":"Flörke"},{"last_name":"Egold","first_name":"Hans","full_name":"Egold, Hans"},{"last_name":"Haupt","first_name":"Hans‐Jürgen","full_name":"Haupt, Hans‐Jürgen"},{"full_name":"Schwefer, Meinhard","last_name":"Schwefer","first_name":"Meinhard"}],"publication_identifier":{"issn":["0044-2313","1521-3749"]},"year":"2005","title":"Synthese und Struktur chiraler Heterometallatetrahedrane des Typs [Re2(M1PPh3)(M2PPh3)(μ‐PCy2)(CO)7C≡CPh] (M1 = Ag, Au; M2 = Cu, Ag, Au)","intvolume":" 632","publication_status":"published","date_updated":"2025-02-12T09:30:52Z","date_created":"2025-02-12T09:26:12Z","department":[{"_id":"321"},{"_id":"35"},{"_id":"301"}],"type":"journal_article","issue":"2","publication":"Zeitschrift für anorganische und allgemeine Chemie","abstract":[{"text":"AbstractSyntheses and Structure of Chiral Metallatetrahedron Complexes of the Type [Re2(M1PPh3)(M2PPh3)(μ‐PCy2)(CO)7C≡CPh] (M1 = Ag, Au; M2 = Cu, Ag, Au)From the reaction of Li[Re2(μ‐H)(μ‐PCy2)(CO)7(C(Ph)O)] (1) with Ph3AuC≡CPh both benzaldehyde and the trinuclear complex Li[Re2(AuPPh3)(μ‐PCy2)(CO)7C≡CPh] (2a) were obtained in high yield. The complex anion was isolated as its PPh4‐salt 2b. The latter reacts with coinage metal complexes PPh3M2Cl [M2 = Cu, Ag, Au] to give chiral heterometallatetrahedranes of the general formula [Re2(AuPPh3)(M2PPh3)(μ‐PCy2)(CO)7C≡CPh] (M2 = Cu 3a, Ag 3b, Au 3c). The corresponding complex [Re2(AgPPh3)2(μ‐PCy2)(CO)7C≡CPh] (3d) is obtained from the reaction of [Re2(AgPPh3)2(μ‐PCy2)(CO)7Cl] (4) with LiC≡CPh. 3d undergoes a metathesis reaction in the presence of PPh3CuCl giving [Re2(AgPPh3)(CuPPh3)(μ‐PCy2)(CO)7C≡CPh] (3e) and PPh3AgCl. Analogous metathesis reactions are observed when 3c is reacted with PPh3AgCl or PPh3CuCl giving 3a or 3b, respectively. The reaction of 1 with PPh3AuCl gives benzaldehyde and Li[Re2(AuPPh3)(μ‐PCy2)(CO)7Cl] (5a) which upon reaction with PhLi forms the trinuclear complex Li[Re2(AuPPh3)(μ‐PCy2)(CO)7Ph] (6a). Again this complex was isolated as its PPh4‐salt 6b. In contrast to 2b, 6b reacts with one equivalent of Ph3PAuCl by transmetalation to give Ph3PAuPh and PPh4[Re2(AuPPh3)(μ‐PCy2)(CO)7Cl] (5b). The X‐ray structures of the compounds 3a, 3b, 3e and 4 are reported.","lang":"eng"}]}]