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The Role of Pd<sup>2+</sup>/Pd<sup>0</sup>in Hydrogenation by [Pd(2-pymo)<sub>2</sub>]<sub><i>n</i></sub>: An X-ray Absorption and IR Spectroscopic Study. <i>Chemistry - A European Journal</i>. 2012;18(49):15831-15837. doi:<a href=\"https://doi.org/10.1002/chem.201202129\">10.1002/chem.201202129</a>"},"page":"15831-15837","_id":"41241","publisher":"Wiley","user_id":"48467","volume":18,"status":"public","date_created":"2023-01-31T14:54:53Z","keyword":["General Chemistry","Catalysis","Organic Chemistry"],"type":"journal_article","department":[{"_id":"306"}],"issue":"49","publication":"Chemistry - A European Journal","language":[{"iso":"eng"}],"doi":"10.1002/chem.201202129","year":"2012","title":"The Role of Pd<sup>2+</sup>/Pd<sup>0</sup>in Hydrogenation by [Pd(2-pymo)<sub>2</sub>]<sub><i>n</i></sub>: An X-ray Absorption and IR Spectroscopic Study","publication_identifier":{"issn":["0947-6539"]},"author":[{"full_name":"Schuster, Sabine","last_name":"Schuster","first_name":"Sabine"},{"full_name":"Klemm, Elias","first_name":"Elias","last_name":"Klemm"},{"full_name":"Bauer, Matthias","first_name":"Matthias","last_name":"Bauer","orcid":"0000-0002-9294-6076","id":"47241"}],"publication_status":"published","date_updated":"2023-01-31T14:55:01Z","intvolume":"        18"},{"publication":"Journal of the American Chemical Society","issue":"10","type":"journal_article","keyword":["Colloid and Surface Chemistry","Biochemistry","General Chemistry","Catalysis"],"department":[{"_id":"306"}],"date_created":"2023-01-31T14:59:48Z","publication_status":"published","date_updated":"2023-01-31T15:00:02Z","intvolume":"       134","year":"2012","title":"Paramagnetic Palladacycles with Pd<sup>III</sup>Centers Are Highly Active Catalysts for Asymmetric Aza-Claisen Rearrangements","author":[{"last_name":"Eitel","first_name":"Simon H.","full_name":"Eitel, Simon H."},{"id":"47241","last_name":"Bauer","orcid":"0000-0002-9294-6076","first_name":"Matthias","full_name":"Bauer, Matthias"},{"full_name":"Schweinfurth, David","first_name":"David","last_name":"Schweinfurth"},{"full_name":"Deibel, Naina","last_name":"Deibel","first_name":"Naina"},{"full_name":"Sarkar, Biprajit","last_name":"Sarkar","first_name":"Biprajit"},{"full_name":"Kelm, Harald","first_name":"Harald","last_name":"Kelm"},{"full_name":"Krüger, Hans-Jörg","last_name":"Krüger","first_name":"Hans-Jörg"},{"last_name":"Frey","first_name":"Wolfgang","full_name":"Frey, Wolfgang"},{"last_name":"Peters","first_name":"René","full_name":"Peters, René"}],"publication_identifier":{"issn":["0002-7863","1520-5126"]},"doi":"10.1021/ja2098222","language":[{"iso":"eng"}],"citation":{"mla":"Eitel, Simon H., et al. “Paramagnetic Palladacycles with Pd<sup>III</sup>Centers Are Highly Active Catalysts for Asymmetric Aza-Claisen Rearrangements.” <i>Journal of the American Chemical Society</i>, vol. 134, no. 10, American Chemical Society (ACS), 2012, pp. 4683–93, doi:<a href=\"https://doi.org/10.1021/ja2098222\">10.1021/ja2098222</a>.","ama":"Eitel SH, Bauer M, Schweinfurth D, et al. 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Comparison is based on the model formfactors of rectangular parallelepipeds, which cover the entire regime of variable wall thickness. The entire regime of wall thicknesses has been made available by the present work, which completed the set of formulas by calculating the formfactor for the limit of hollow parallelepipeds with infinitely thin walls, which was still lacking. The formfactors are expressed as a function of the momentum transfer<jats:italic>q</jats:italic>. Discrimination between massive and hollow structures by means of the<jats:italic>q</jats:italic>-dependent scattering data<jats:italic>SF(q)</jats:italic>gets possible once the Guinier radius and the particle volume can be established at the lower limit of<jats:italic>q</jats:italic>or a power law of<jats:italic>SF(q)</jats:italic>∼<jats:italic>q</jats:italic><jats:sup><jats:italic>α</jats:italic></jats:sup>can be extracted towards large<jats:italic>q</jats:italic>. Whereas the former requires extrapolation of the scattering data to<jats:italic>q</jats:italic>= 0 with high accuracy, the latter needs experiments over a very broad<jats:italic>q</jats:italic>-regime. If experimental data is restricted to a<jats:italic>q</jats:italic>-regime which includes only the first peak in a Kratky representation of<jats:italic>q</jats:italic><jats:sup>2</jats:sup><jats:italic>SF(q)</jats:italic><jats:italic>vs.</jats:italic><jats:italic>q</jats:italic>without giving way to an accurate extrapolation to<jats:italic>q</jats:italic>= 0 nor to a clear power law in<jats:italic>q</jats:italic>, discrimination between a hollow and a massive structure gets extremely difficult. Yet, the effect of anisometry is striking and enables extraction of a crude guess of the degree of anisometry already from the first Kratky peak. This could be achieved by introducing a dimensionless parameter established from the width and location of the first Kratky peak.</jats:p>","lang":"eng"}],"language":[{"iso":"eng"}],"doi":"10.1524/zpch.2012.0257","author":[{"full_name":"Nayuk, Roman","first_name":"Roman","last_name":"Nayuk"},{"full_name":"Huber, Klaus","last_name":"Huber","first_name":"Klaus","id":"237"}],"publication_identifier":{"issn":["2196-7156","0942-9352"]},"title":"Formfactors of Hollow and Massive Rectangular Parallelepipeds at Variable Degree of Anisometry","year":"2012","intvolume":"       226","publication_status":"published","date_updated":"2023-02-10T14:24:25Z","citation":{"apa":"Nayuk, R., &#38; Huber, K. (2012). Formfactors of Hollow and Massive Rectangular Parallelepipeds at Variable Degree of Anisometry. <i>Zeitschrift Für Physikalische Chemie</i>, <i>226</i>(7–8), 837–854. <a href=\"https://doi.org/10.1524/zpch.2012.0257\">https://doi.org/10.1524/zpch.2012.0257</a>","ieee":"R. Nayuk and K. Huber, “Formfactors of Hollow and Massive Rectangular Parallelepipeds at Variable Degree of Anisometry,” <i>Zeitschrift für Physikalische Chemie</i>, vol. 226, no. 7–8, pp. 837–854, 2012, doi: <a href=\"https://doi.org/10.1524/zpch.2012.0257\">10.1524/zpch.2012.0257</a>.","short":"R. Nayuk, K. 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Formfactors of Hollow and Massive Rectangular Parallelepipeds at Variable Degree of Anisometry. <i>Zeitschrift für Physikalische Chemie</i>. 2012;226(7-8):837-854. doi:<a href=\"https://doi.org/10.1524/zpch.2012.0257\">10.1524/zpch.2012.0257</a>","bibtex":"@article{Nayuk_Huber_2012, title={Formfactors of Hollow and Massive Rectangular Parallelepipeds at Variable Degree of Anisometry}, volume={226}, DOI={<a href=\"https://doi.org/10.1524/zpch.2012.0257\">10.1524/zpch.2012.0257</a>}, number={7–8}, journal={Zeitschrift für Physikalische Chemie}, publisher={Walter de Gruyter GmbH}, author={Nayuk, Roman and Huber, Klaus}, year={2012}, pages={837–854} }"},"_id":"41983","publisher":"Walter de Gruyter GmbH","page":"837-854","volume":226,"user_id":"237","status":"public"},{"page":"3593-3605","publisher":"American Chemical Society (ACS)","_id":"41985","user_id":"237","volume":28,"status":"public","citation":{"apa":"Liu, J., Pancera, S., Boyko, V., Gummel, J., Nayuk, R., &#38; Huber, K. (2012). Impact of Sodium Polyacrylate on the Amorphous Calcium Carbonate Formation from Supersaturated Solution. <i>Langmuir</i>, <i>28</i>(7), 3593–3605. <a href=\"https://doi.org/10.1021/la203895d\">https://doi.org/10.1021/la203895d</a>","ieee":"J. Liu, S. Pancera, V. Boyko, J. Gummel, R. Nayuk, and K. Huber, “Impact of Sodium Polyacrylate on the Amorphous Calcium Carbonate Formation from Supersaturated Solution,” <i>Langmuir</i>, vol. 28, no. 7, pp. 3593–3605, 2012, doi: <a href=\"https://doi.org/10.1021/la203895d\">10.1021/la203895d</a>.","short":"J. Liu, S. Pancera, V. Boyko, J. Gummel, R. Nayuk, K. Huber, Langmuir 28 (2012) 3593–3605.","chicago":"Liu, J., S. Pancera, V. Boyko, J. Gummel, R. Nayuk, and Klaus Huber. “Impact of Sodium Polyacrylate on the Amorphous Calcium Carbonate Formation from Supersaturated Solution.” <i>Langmuir</i> 28, no. 7 (2012): 3593–3605. <a href=\"https://doi.org/10.1021/la203895d\">https://doi.org/10.1021/la203895d</a>.","mla":"Liu, J., et al. “Impact of Sodium Polyacrylate on the Amorphous Calcium Carbonate Formation from Supersaturated Solution.” <i>Langmuir</i>, vol. 28, no. 7, American Chemical Society (ACS), 2012, pp. 3593–605, doi:<a href=\"https://doi.org/10.1021/la203895d\">10.1021/la203895d</a>.","ama":"Liu J, Pancera S, Boyko V, Gummel J, Nayuk R, Huber K. Impact of Sodium Polyacrylate on the Amorphous Calcium Carbonate Formation from Supersaturated Solution. <i>Langmuir</i>. 2012;28(7):3593-3605. doi:<a href=\"https://doi.org/10.1021/la203895d\">10.1021/la203895d</a>","bibtex":"@article{Liu_Pancera_Boyko_Gummel_Nayuk_Huber_2012, title={Impact of Sodium Polyacrylate on the Amorphous Calcium Carbonate Formation from Supersaturated Solution}, volume={28}, DOI={<a href=\"https://doi.org/10.1021/la203895d\">10.1021/la203895d</a>}, number={7}, journal={Langmuir}, publisher={American Chemical Society (ACS)}, author={Liu, J. and Pancera, S. and Boyko, V. and Gummel, J. and Nayuk, R. and Huber, Klaus}, year={2012}, pages={3593–3605} }"},"language":[{"iso":"eng"}],"doi":"10.1021/la203895d","title":"Impact of Sodium Polyacrylate on the Amorphous Calcium Carbonate Formation from Supersaturated Solution","year":"2012","publication_identifier":{"issn":["0743-7463","1520-5827"]},"author":[{"last_name":"Liu","first_name":"J.","full_name":"Liu, J."},{"first_name":"S.","last_name":"Pancera","full_name":"Pancera, S."},{"full_name":"Boyko, V.","last_name":"Boyko","first_name":"V."},{"last_name":"Gummel","first_name":"J.","full_name":"Gummel, J."},{"full_name":"Nayuk, R.","last_name":"Nayuk","first_name":"R."},{"last_name":"Huber","first_name":"Klaus","full_name":"Huber, Klaus","id":"237"}],"date_updated":"2023-02-10T14:26:34Z","publication_status":"published","intvolume":"        28","date_created":"2023-02-10T14:26:07Z","type":"journal_article","keyword":["Electrochemistry","Spectroscopy","Surfaces and Interfaces","Condensed Matter Physics","General Materials Science"],"department":[{"_id":"314"}],"publication":"Langmuir","issue":"7"},{"status":"public","user_id":"237","volume":116,"page":"6127-6135","_id":"41984","publisher":"American Chemical Society (ACS)","citation":{"ieee":"R. 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