---
_id: '43441'
abstract:
- lang: eng
  text: "This paper reveals the 3D character of the intermetallic layer at the aluminum–steel
    interface which pops\r\nup above the original sample surface during annealing.
    Popping out of the intermetallics was proven using\r\natomic force microscopy.
    The phase expands out of the plane due to the exothermic formation of the Al5Fe2\r\nphase
    and the feasibility of surface diffusion. Milling by a focused ion beam enabled
    the comparison of the\r\nchemical composition of the surface layer with the bulk
    interface, showing no difference. The growth direction\r\nis both towards aluminum
    and steel — the main diffusion flux is from aluminum towards steel, and the new\r\nintermetallic
    phase emerges at the steel side. The shortage of Al atoms causes a shift of the
    intermetallic as a\r\nwhole towards aluminum."
article_number: '112043'
article_type: original
author:
- first_name: Michaela
  full_name: Šlapáková, Michaela
  last_name: Šlapáková
- first_name: Barbora
  full_name: Kihoulou, Barbora
  last_name: Kihoulou
- first_name: Jozef
  full_name: Veselý, Jozef
  last_name: Veselý
- first_name: Peter
  full_name: Minárik, Peter
  last_name: Minárik
- first_name: Klaudia
  full_name: Fekete, Klaudia
  last_name: Fekete
- first_name: Michal
  full_name: Knapek, Michal
  last_name: Knapek
- first_name: Rostislav
  full_name: Králík, Rostislav
  last_name: Králík
- first_name: Olexandr
  full_name: Grydin, Olexandr
  id: '43822'
  last_name: Grydin
- first_name: Mykhailo
  full_name: Stolbchenko, Mykhailo
  last_name: Stolbchenko
- first_name: Mirko
  full_name: Schaper, Mirko
  id: '43720'
  last_name: Schaper
citation:
  ama: Šlapáková M, Kihoulou B, Veselý J, et al. 3D-structure of intermetallic interface
    layer in Al–steel clad material. <i>Vacuum</i>. 2023;212. doi:<a href="https://doi.org/10.1016/j.vacuum.2023.112043">10.1016/j.vacuum.2023.112043</a>
  apa: Šlapáková, M., Kihoulou, B., Veselý, J., Minárik, P., Fekete, K., Knapek, M.,
    Králík, R., Grydin, O., Stolbchenko, M., &#38; Schaper, M. (2023). 3D-structure
    of intermetallic interface layer in Al–steel clad material. <i>Vacuum</i>, <i>212</i>,
    Article 112043. <a href="https://doi.org/10.1016/j.vacuum.2023.112043">https://doi.org/10.1016/j.vacuum.2023.112043</a>
  bibtex: '@article{Šlapáková_Kihoulou_Veselý_Minárik_Fekete_Knapek_Králík_Grydin_Stolbchenko_Schaper_2023,
    title={3D-structure of intermetallic interface layer in Al–steel clad material},
    volume={212}, DOI={<a href="https://doi.org/10.1016/j.vacuum.2023.112043">10.1016/j.vacuum.2023.112043</a>},
    number={112043}, journal={Vacuum}, publisher={Elsevier BV}, author={Šlapáková,
    Michaela and Kihoulou, Barbora and Veselý, Jozef and Minárik, Peter and Fekete,
    Klaudia and Knapek, Michal and Králík, Rostislav and Grydin, Olexandr and Stolbchenko,
    Mykhailo and Schaper, Mirko}, year={2023} }'
  chicago: Šlapáková, Michaela, Barbora Kihoulou, Jozef Veselý, Peter Minárik, Klaudia
    Fekete, Michal Knapek, Rostislav Králík, Olexandr Grydin, Mykhailo Stolbchenko,
    and Mirko Schaper. “3D-Structure of Intermetallic Interface Layer in Al–Steel
    Clad Material.” <i>Vacuum</i> 212 (2023). <a href="https://doi.org/10.1016/j.vacuum.2023.112043">https://doi.org/10.1016/j.vacuum.2023.112043</a>.
  ieee: 'M. Šlapáková <i>et al.</i>, “3D-structure of intermetallic interface layer
    in Al–steel clad material,” <i>Vacuum</i>, vol. 212, Art. no. 112043, 2023, doi:
    <a href="https://doi.org/10.1016/j.vacuum.2023.112043">10.1016/j.vacuum.2023.112043</a>.'
  mla: Šlapáková, Michaela, et al. “3D-Structure of Intermetallic Interface Layer
    in Al–Steel Clad Material.” <i>Vacuum</i>, vol. 212, 112043, Elsevier BV, 2023,
    doi:<a href="https://doi.org/10.1016/j.vacuum.2023.112043">10.1016/j.vacuum.2023.112043</a>.
  short: M. Šlapáková, B. Kihoulou, J. Veselý, P. Minárik, K. Fekete, M. Knapek, R.
    Králík, O. Grydin, M. Stolbchenko, M. Schaper, Vacuum 212 (2023).
date_created: 2023-04-08T17:24:40Z
date_updated: 2023-06-01T14:22:15Z
department:
- _id: '158'
doi: 10.1016/j.vacuum.2023.112043
intvolume: '       212'
keyword:
- Al-steel clad
- twin-roll casting
- 3D characterization
- atomic force microscopy
- diffusion direction
- surface growth
language:
- iso: eng
publication: Vacuum
publication_identifier:
  issn:
  - 0042-207X
publication_status: published
publisher: Elsevier BV
quality_controlled: '1'
status: public
title: 3D-structure of intermetallic interface layer in Al–steel clad material
type: journal_article
user_id: '43720'
volume: 212
year: '2023'
...
---
_id: '22622'
author:
- first_name: I.
  full_name: Tanarro, I.
  last_name: Tanarro
- first_name: Maria Teresa
  full_name: de los Arcos de Pedro, Maria Teresa
  id: '54556'
  last_name: de los Arcos de Pedro
- first_name: C.
  full_name: Domingo, C.
  last_name: Domingo
- first_name: V.J.
  full_name: Herrero, V.J.
  last_name: Herrero
- first_name: M.M.
  full_name: Sanz, M.M.
  last_name: Sanz
citation:
  ama: Tanarro I, de los Arcos de Pedro MT, Domingo C, Herrero VJ, Sanz MM. Diagnostics
    and modeling of glow discharges by time-resolved IR absorption spectroscopy. <i>Vacuum</i>.
    Published online 2002:457-465. doi:<a href="https://doi.org/10.1016/s0042-207x(01)00338-4">10.1016/s0042-207x(01)00338-4</a>
  apa: Tanarro, I., de los Arcos de Pedro, M. T., Domingo, C., Herrero, V. J., &#38;
    Sanz, M. M. (2002). Diagnostics and modeling of glow discharges by time-resolved
    IR absorption spectroscopy. <i>Vacuum</i>, 457–465. <a href="https://doi.org/10.1016/s0042-207x(01)00338-4">https://doi.org/10.1016/s0042-207x(01)00338-4</a>
  bibtex: '@article{Tanarro_de los Arcos de Pedro_Domingo_Herrero_Sanz_2002, title={Diagnostics
    and modeling of glow discharges by time-resolved IR absorption spectroscopy},
    DOI={<a href="https://doi.org/10.1016/s0042-207x(01)00338-4">10.1016/s0042-207x(01)00338-4</a>},
    journal={Vacuum}, author={Tanarro, I. and de los Arcos de Pedro, Maria Teresa
    and Domingo, C. and Herrero, V.J. and Sanz, M.M.}, year={2002}, pages={457–465}
    }'
  chicago: Tanarro, I., Maria Teresa de los Arcos de Pedro, C. Domingo, V.J. Herrero,
    and M.M. Sanz. “Diagnostics and Modeling of Glow Discharges by Time-Resolved IR
    Absorption Spectroscopy.” <i>Vacuum</i>, 2002, 457–65. <a href="https://doi.org/10.1016/s0042-207x(01)00338-4">https://doi.org/10.1016/s0042-207x(01)00338-4</a>.
  ieee: 'I. Tanarro, M. T. de los Arcos de Pedro, C. Domingo, V. J. Herrero, and M.
    M. Sanz, “Diagnostics and modeling of glow discharges by time-resolved IR absorption
    spectroscopy,” <i>Vacuum</i>, pp. 457–465, 2002, doi: <a href="https://doi.org/10.1016/s0042-207x(01)00338-4">10.1016/s0042-207x(01)00338-4</a>.'
  mla: Tanarro, I., et al. “Diagnostics and Modeling of Glow Discharges by Time-Resolved
    IR Absorption Spectroscopy.” <i>Vacuum</i>, 2002, pp. 457–65, doi:<a href="https://doi.org/10.1016/s0042-207x(01)00338-4">10.1016/s0042-207x(01)00338-4</a>.
  short: I. Tanarro, M.T. de los Arcos de Pedro, C. Domingo, V.J. Herrero, M.M. Sanz,
    Vacuum (2002) 457–465.
date_created: 2021-07-07T11:49:16Z
date_updated: 2023-01-24T08:31:23Z
department:
- _id: '302'
doi: 10.1016/s0042-207x(01)00338-4
extern: '1'
language:
- iso: eng
page: 457-465
publication: Vacuum
publication_identifier:
  issn:
  - 0042-207X
publication_status: published
status: public
title: Diagnostics and modeling of glow discharges by time-resolved IR absorption
  spectroscopy
type: journal_article
user_id: '54556'
year: '2002'
...
---
_id: '22619'
author:
- first_name: Maria Teresa
  full_name: de los Arcos de Pedro, Maria Teresa
  id: '54556'
  last_name: de los Arcos de Pedro
- first_name: P
  full_name: Oelhafen, P
  last_name: Oelhafen
- first_name: U
  full_name: Aebi, U
  last_name: Aebi
- first_name: A
  full_name: Hefti, A
  last_name: Hefti
- first_name: M
  full_name: Düggelin, M
  last_name: Düggelin
- first_name: D
  full_name: Mathys, D
  last_name: Mathys
- first_name: R
  full_name: Guggenheim, R
  last_name: Guggenheim
citation:
  ama: de los Arcos de Pedro MT, Oelhafen P, Aebi U, et al. Preparation and characterization
    of TiN–Ag nanocomposite films. <i>Vacuum</i>. Published online 2002:463-470. doi:<a
    href="https://doi.org/10.1016/s0042-207x(02)00232-4">10.1016/s0042-207x(02)00232-4</a>
  apa: de los Arcos de Pedro, M. T., Oelhafen, P., Aebi, U., Hefti, A., Düggelin,
    M., Mathys, D., &#38; Guggenheim, R. (2002). Preparation and characterization
    of TiN–Ag nanocomposite films. <i>Vacuum</i>, 463–470. <a href="https://doi.org/10.1016/s0042-207x(02)00232-4">https://doi.org/10.1016/s0042-207x(02)00232-4</a>
  bibtex: '@article{de los Arcos de Pedro_Oelhafen_Aebi_Hefti_Düggelin_Mathys_Guggenheim_2002,
    title={Preparation and characterization of TiN–Ag nanocomposite films}, DOI={<a
    href="https://doi.org/10.1016/s0042-207x(02)00232-4">10.1016/s0042-207x(02)00232-4</a>},
    journal={Vacuum}, author={de los Arcos de Pedro, Maria Teresa and Oelhafen, P
    and Aebi, U and Hefti, A and Düggelin, M and Mathys, D and Guggenheim, R}, year={2002},
    pages={463–470} }'
  chicago: Arcos de Pedro, Maria Teresa de los, P Oelhafen, U Aebi, A Hefti, M Düggelin,
    D Mathys, and R Guggenheim. “Preparation and Characterization of TiN–Ag Nanocomposite
    Films.” <i>Vacuum</i>, 2002, 463–70. <a href="https://doi.org/10.1016/s0042-207x(02)00232-4">https://doi.org/10.1016/s0042-207x(02)00232-4</a>.
  ieee: 'M. T. de los Arcos de Pedro <i>et al.</i>, “Preparation and characterization
    of TiN–Ag nanocomposite films,” <i>Vacuum</i>, pp. 463–470, 2002, doi: <a href="https://doi.org/10.1016/s0042-207x(02)00232-4">10.1016/s0042-207x(02)00232-4</a>.'
  mla: de los Arcos de Pedro, Maria Teresa, et al. “Preparation and Characterization
    of TiN–Ag Nanocomposite Films.” <i>Vacuum</i>, 2002, pp. 463–70, doi:<a href="https://doi.org/10.1016/s0042-207x(02)00232-4">10.1016/s0042-207x(02)00232-4</a>.
  short: M.T. de los Arcos de Pedro, P. Oelhafen, U. Aebi, A. Hefti, M. Düggelin,
    D. Mathys, R. Guggenheim, Vacuum (2002) 463–470.
date_created: 2021-07-07T11:46:08Z
date_updated: 2023-01-24T08:30:40Z
department:
- _id: '302'
doi: 10.1016/s0042-207x(02)00232-4
extern: '1'
language:
- iso: eng
page: 463-470
publication: Vacuum
publication_identifier:
  issn:
  - 0042-207X
publication_status: published
status: public
title: Preparation and characterization of TiN–Ag nanocomposite films
type: journal_article
user_id: '54556'
year: '2002'
...