---
_id: '51145'
author:
- first_name: Orlando
full_name: Massopo, Orlando
id: '98419'
last_name: Massopo
- first_name: Hans-Joachim
full_name: Schmid, Hans-Joachim
id: '464'
last_name: Schmid
orcid: 000-0001-8590-1921
- first_name: Munko
full_name: Gonchikzhapov, Munko
id: '94996'
last_name: Gonchikzhapov
orcid: https://orcid.org/0000-0002-7773-047X
- first_name: Tina
full_name: Kasper, Tina
id: '94562'
last_name: Kasper
orcid: '0000-0003-3993-5316 '
citation:
ama: 'Massopo O, Schmid H-J, Gonchikzhapov M, Kasper T. Nanoparticle Concentration
Measurement in Flame Spray Pyrolysis (Poster). In: ; 2023.'
apa: Massopo, O., Schmid, H.-J., Gonchikzhapov, M., & Kasper, T. (2023). Nanoparticle
Concentration Measurement in Flame Spray Pyrolysis (Poster). European Aerosol
Conference, Málaga, Spain .
bibtex: '@inproceedings{Massopo_Schmid_Gonchikzhapov_Kasper_2023, title={Nanoparticle
Concentration Measurement in Flame Spray Pyrolysis (Poster)}, author={Massopo,
Orlando and Schmid, Hans-Joachim and Gonchikzhapov, Munko and Kasper, Tina}, year={2023}
}'
chicago: Massopo, Orlando, Hans-Joachim Schmid, Munko Gonchikzhapov, and Tina Kasper.
“Nanoparticle Concentration Measurement in Flame Spray Pyrolysis (Poster),” 2023.
ieee: O. Massopo, H.-J. Schmid, M. Gonchikzhapov, and T. Kasper, “Nanoparticle Concentration
Measurement in Flame Spray Pyrolysis (Poster),” presented at the European Aerosol
Conference, Málaga, Spain , 2023.
mla: Massopo, Orlando, et al. Nanoparticle Concentration Measurement in Flame
Spray Pyrolysis (Poster). 2023.
short: 'O. Massopo, H.-J. Schmid, M. Gonchikzhapov, T. Kasper, in: 2023.'
conference:
end_date: 2023-09-08
location: 'Málaga, Spain '
name: European Aerosol Conference
start_date: 2023-09-03
date_created: 2024-02-05T12:45:55Z
date_updated: 2024-02-05T12:46:11Z
department:
- _id: '150'
- _id: '728'
keyword:
- Absolute particle concentration
- Flame Spray Pyrolysis
- SMPS
- Mass Spectrometry
language:
- iso: eng
status: public
title: Nanoparticle Concentration Measurement in Flame Spray Pyrolysis (Poster)
type: conference_abstract
user_id: '98419'
year: '2023'
...
---
_id: '45602'
article_number: '100152'
author:
- first_name: Yasin
full_name: Karakaya, Yasin
id: '95069'
last_name: Karakaya
- first_name: H.
full_name: Somnitz, H.
last_name: Somnitz
- first_name: A.
full_name: Hermsen, A.
last_name: Hermsen
- first_name: Munko
full_name: Gonchikzhapov, Munko
id: '94996'
last_name: Gonchikzhapov
orcid: https://orcid.org/0000-0002-7773-047X
- first_name: Tina
full_name: Kasper, Tina
id: '94562'
last_name: Kasper
orcid: '0000-0003-3993-5316 '
citation:
ama: Karakaya Y, Somnitz H, Hermsen A, Gonchikzhapov M, Kasper T. Revisiting the
initial reaction rates for TMS combustion and a new evidence for metastable silica
nanoparticles in the gas-phase synthesis. Applications in Energy and Combustion
Science. 2023;14. doi:10.1016/j.jaecs.2023.100152
apa: Karakaya, Y., Somnitz, H., Hermsen, A., Gonchikzhapov, M., & Kasper, T.
(2023). Revisiting the initial reaction rates for TMS combustion and a new evidence
for metastable silica nanoparticles in the gas-phase synthesis. Applications
in Energy and Combustion Science, 14, Article 100152. https://doi.org/10.1016/j.jaecs.2023.100152
bibtex: '@article{Karakaya_Somnitz_Hermsen_Gonchikzhapov_Kasper_2023, title={Revisiting
the initial reaction rates for TMS combustion and a new evidence for metastable
silica nanoparticles in the gas-phase synthesis}, volume={14}, DOI={10.1016/j.jaecs.2023.100152},
number={100152}, journal={Applications in Energy and Combustion Science}, publisher={Elsevier
BV}, author={Karakaya, Yasin and Somnitz, H. and Hermsen, A. and Gonchikzhapov,
Munko and Kasper, Tina}, year={2023} }'
chicago: Karakaya, Yasin, H. Somnitz, A. Hermsen, Munko Gonchikzhapov, and Tina
Kasper. “Revisiting the Initial Reaction Rates for TMS Combustion and a New Evidence
for Metastable Silica Nanoparticles in the Gas-Phase Synthesis.” Applications
in Energy and Combustion Science 14 (2023). https://doi.org/10.1016/j.jaecs.2023.100152.
ieee: 'Y. Karakaya, H. Somnitz, A. Hermsen, M. Gonchikzhapov, and T. Kasper, “Revisiting
the initial reaction rates for TMS combustion and a new evidence for metastable
silica nanoparticles in the gas-phase synthesis,” Applications in Energy and
Combustion Science, vol. 14, Art. no. 100152, 2023, doi: 10.1016/j.jaecs.2023.100152.'
mla: Karakaya, Yasin, et al. “Revisiting the Initial Reaction Rates for TMS Combustion
and a New Evidence for Metastable Silica Nanoparticles in the Gas-Phase Synthesis.”
Applications in Energy and Combustion Science, vol. 14, 100152, Elsevier
BV, 2023, doi:10.1016/j.jaecs.2023.100152.
short: Y. Karakaya, H. Somnitz, A. Hermsen, M. Gonchikzhapov, T. Kasper, Applications
in Energy and Combustion Science 14 (2023).
date_created: 2023-06-13T18:32:33Z
date_updated: 2023-08-22T20:03:29Z
department:
- _id: '728'
doi: 10.1016/j.jaecs.2023.100152
intvolume: ' 14'
keyword:
- Metastable particles
- Nanomaterials
- Quartz-crystal-microbalance
- Molecular-beam mass spectrometry
- Tetramethylsilane
- Reaction kinetics
language:
- iso: eng
main_file_link:
- open_access: '1'
url: https://www.sciencedirect.com/science/article/pii/S2666352X23000419
oa: '1'
publication: Applications in Energy and Combustion Science
publication_identifier:
issn:
- 2666-352X
publication_status: published
publisher: Elsevier BV
quality_controlled: '1'
status: public
title: Revisiting the initial reaction rates for TMS combustion and a new evidence
for metastable silica nanoparticles in the gas-phase synthesis
type: journal_article
user_id: '94996'
volume: 14
year: '2023'
...
---
_id: '32416'
abstract:
- lang: eng
text: In recent years, sequence-defined oligomers (SDOs) gained increasing interest
due to their perfectly controlled molecular structure, thus providing defined
properties. In order to tune the properties, different functionalities need to
be incorporated into the oligomers and the chain tacticity needs to be controlled.
Beside the synthesis of SDOs, suitable methods need to be found to analyze the
molecular structure. In this work, oligomers exhibiting an alternating or block-wise
sequence of side chain functionalities were analyzed using a hyphenation of ultra-high-performance
liquid chromatography and electrospray ionization mass spectrometry enhanced by
ion mobility separation (IMS). Moieties in the side chains were varied according
to polarity and bulkiness. Moreover, chain tacticity was varied. Drift times in
the IMS cell and the corresponding collision cross section (CCS) values were shown
to be individual parameters allowing the identification of SDOs, even in the case
that SDO structures only differ in sequence or tacticity of side chain functionalities.
Thus, a library of CCS values was obtained as reference used for the analysis
of complex mixtures of SDOs.
article_type: original
author:
- first_name: Marie-Theres
full_name: Berg, Marie-Theres
last_name: Berg
- first_name: Artjom
full_name: Herberg, Artjom
id: '94'
last_name: Herberg
- first_name: Dirk
full_name: Kuckling, Dirk
id: '287'
last_name: Kuckling
citation:
ama: Berg M-T, Herberg A, Kuckling D. Hyphenation of ultra-high-performance liquid
chromatography and ion mobility mass spectrometry for the analysis of sequence-defined
oligomers with different functionalities and tacticity. International Journal
of Polymer Analysis and Characterization. Published online 2022:1-12. doi:10.1080/1023666x.2022.2100968
apa: Berg, M.-T., Herberg, A., & Kuckling, D. (2022). Hyphenation of ultra-high-performance
liquid chromatography and ion mobility mass spectrometry for the analysis of sequence-defined
oligomers with different functionalities and tacticity. International Journal
of Polymer Analysis and Characterization, 1–12. https://doi.org/10.1080/1023666x.2022.2100968
bibtex: '@article{Berg_Herberg_Kuckling_2022, title={Hyphenation of ultra-high-performance
liquid chromatography and ion mobility mass spectrometry for the analysis of sequence-defined
oligomers with different functionalities and tacticity}, DOI={10.1080/1023666x.2022.2100968},
journal={International Journal of Polymer Analysis and Characterization}, publisher={Informa
UK Limited}, author={Berg, Marie-Theres and Herberg, Artjom and Kuckling, Dirk},
year={2022}, pages={1–12} }'
chicago: Berg, Marie-Theres, Artjom Herberg, and Dirk Kuckling. “Hyphenation of
Ultra-High-Performance Liquid Chromatography and Ion Mobility Mass Spectrometry
for the Analysis of Sequence-Defined Oligomers with Different Functionalities
and Tacticity.” International Journal of Polymer Analysis and Characterization,
2022, 1–12. https://doi.org/10.1080/1023666x.2022.2100968.
ieee: 'M.-T. Berg, A. Herberg, and D. Kuckling, “Hyphenation of ultra-high-performance
liquid chromatography and ion mobility mass spectrometry for the analysis of sequence-defined
oligomers with different functionalities and tacticity,” International Journal
of Polymer Analysis and Characterization, pp. 1–12, 2022, doi: 10.1080/1023666x.2022.2100968.'
mla: Berg, Marie-Theres, et al. “Hyphenation of Ultra-High-Performance Liquid Chromatography
and Ion Mobility Mass Spectrometry for the Analysis of Sequence-Defined Oligomers
with Different Functionalities and Tacticity.” International Journal of Polymer
Analysis and Characterization, Informa UK Limited, 2022, pp. 1–12, doi:10.1080/1023666x.2022.2100968.
short: M.-T. Berg, A. Herberg, D. Kuckling, International Journal of Polymer Analysis
and Characterization (2022) 1–12.
date_created: 2022-07-26T06:38:52Z
date_updated: 2023-01-10T08:14:52Z
department:
- _id: '163'
doi: 10.1080/1023666x.2022.2100968
keyword:
- Ultra-high-performance liquid chromatography
- ion mobility separation
- mass spectrometry
- LC-MS hyphenation
- sequence-defined oligomers
language:
- iso: eng
page: 1-12
publication: International Journal of Polymer Analysis and Characterization
publication_identifier:
issn:
- 1023-666X
- 1563-5341
publication_status: published
publisher: Informa UK Limited
status: public
title: Hyphenation of ultra-high-performance liquid chromatography and ion mobility
mass spectrometry for the analysis of sequence-defined oligomers with different
functionalities and tacticity
type: journal_article
user_id: '94'
year: '2022'
...
---
_id: '44375'
author:
- first_name: Dotse Selali
full_name: Chormey, Dotse Selali
last_name: Chormey
- first_name: Güldeniz
full_name: Tonbul, Güldeniz
id: '89054'
last_name: Tonbul
orcid: 0000-0002-0999-9995
- first_name: Güneş
full_name: Soylu, Güneş
last_name: Soylu
- first_name: Ahmet
full_name: Saygılar, Ahmet
last_name: Saygılar
- first_name: Sezgin
full_name: Bakırdere, Sezgin
last_name: Bakırdere
citation:
ama: Chormey DS, Tonbul G, Soylu G, Saygılar A, Bakırdere S. Determination of Four
Priority Polycyclic Aromatic Hydrocarbons in Food Samples by Gas Chromatography
– Mass Spectrometry (GC-MS) after Vortex Assisted Dispersive Liquid-Liquid Microextraction
(DLLME). Analytical Letters. 2021;55(2):237-245. doi:10.1080/00032719.2021.1922432
apa: Chormey, D. S., Tonbul, G., Soylu, G., Saygılar, A., & Bakırdere, S. (2021).
Determination of Four Priority Polycyclic Aromatic Hydrocarbons in Food Samples
by Gas Chromatography – Mass Spectrometry (GC-MS) after Vortex Assisted Dispersive
Liquid-Liquid Microextraction (DLLME). Analytical Letters, 55(2),
237–245. https://doi.org/10.1080/00032719.2021.1922432
bibtex: '@article{Chormey_Tonbul_Soylu_Saygılar_Bakırdere_2021, title={Determination
of Four Priority Polycyclic Aromatic Hydrocarbons in Food Samples by Gas Chromatography
– Mass Spectrometry (GC-MS) after Vortex Assisted Dispersive Liquid-Liquid Microextraction
(DLLME)}, volume={55}, DOI={10.1080/00032719.2021.1922432},
number={2}, journal={Analytical Letters}, publisher={Informa UK Limited}, author={Chormey,
Dotse Selali and Tonbul, Güldeniz and Soylu, Güneş and Saygılar, Ahmet and Bakırdere,
Sezgin}, year={2021}, pages={237–245} }'
chicago: 'Chormey, Dotse Selali, Güldeniz Tonbul, Güneş Soylu, Ahmet Saygılar, and
Sezgin Bakırdere. “Determination of Four Priority Polycyclic Aromatic Hydrocarbons
in Food Samples by Gas Chromatography – Mass Spectrometry (GC-MS) after Vortex
Assisted Dispersive Liquid-Liquid Microextraction (DLLME).” Analytical Letters
55, no. 2 (2021): 237–45. https://doi.org/10.1080/00032719.2021.1922432.'
ieee: 'D. S. Chormey, G. Tonbul, G. Soylu, A. Saygılar, and S. Bakırdere, “Determination
of Four Priority Polycyclic Aromatic Hydrocarbons in Food Samples by Gas Chromatography
– Mass Spectrometry (GC-MS) after Vortex Assisted Dispersive Liquid-Liquid Microextraction
(DLLME),” Analytical Letters, vol. 55, no. 2, pp. 237–245, 2021, doi: 10.1080/00032719.2021.1922432.'
mla: Chormey, Dotse Selali, et al. “Determination of Four Priority Polycyclic Aromatic
Hydrocarbons in Food Samples by Gas Chromatography – Mass Spectrometry (GC-MS)
after Vortex Assisted Dispersive Liquid-Liquid Microextraction (DLLME).” Analytical
Letters, vol. 55, no. 2, Informa UK Limited, 2021, pp. 237–45, doi:10.1080/00032719.2021.1922432.
short: D.S. Chormey, G. Tonbul, G. Soylu, A. Saygılar, S. Bakırdere, Analytical
Letters 55 (2021) 237–245.
date_created: 2023-05-03T08:13:58Z
date_updated: 2023-05-03T08:26:30Z
doi: 10.1080/00032719.2021.1922432
intvolume: ' 55'
issue: '2'
keyword:
- Dispersive liquid-liquid microextraction (DLLME)
- gas chromatography – mass spectrometry (GC-MS)
- polycyclic aromatic hydrocarbons
- QuEChERS
language:
- iso: eng
page: 237-245
publication: Analytical Letters
publication_identifier:
issn:
- 0003-2719
- 1532-236X
publication_status: published
publisher: Informa UK Limited
status: public
title: Determination of Four Priority Polycyclic Aromatic Hydrocarbons in Food Samples
by Gas Chromatography – Mass Spectrometry (GC-MS) after Vortex Assisted Dispersive
Liquid-Liquid Microextraction (DLLME)
type: journal_article
user_id: '89054'
volume: 55
year: '2021'
...
---
_id: '30932'
article_number: '678'
author:
- first_name: Artjom
full_name: Herberg, Artjom
id: '94'
last_name: Herberg
- first_name: Xiaoqian
full_name: Yu, Xiaoqian
last_name: Yu
- first_name: Dirk
full_name: Kuckling, Dirk
id: '287'
last_name: Kuckling
citation:
ama: 'Herberg A, Yu X, Kuckling D. End Group Stability of Atom Transfer Radical
Polymerization (ATRP)-Synthesized Poly(N-isopropylacrylamide): Perspectives for
Diblock Copolymer Synthesis. Polymers. 2019;11(4). doi:https://doi.org/10.3390/polym11040678'
apa: 'Herberg, A., Yu, X., & Kuckling, D. (2019). End Group Stability of Atom
Transfer Radical Polymerization (ATRP)-Synthesized Poly(N-isopropylacrylamide):
Perspectives for Diblock Copolymer Synthesis. Polymers, 11(4), Article
678. https://doi.org/10.3390/polym11040678'
bibtex: '@article{Herberg_Yu_Kuckling_2019, title={End Group Stability of Atom Transfer
Radical Polymerization (ATRP)-Synthesized Poly(N-isopropylacrylamide): Perspectives
for Diblock Copolymer Synthesis}, volume={11}, DOI={https://doi.org/10.3390/polym11040678},
number={4678}, journal={Polymers}, publisher={MDPI}, author={Herberg, Artjom and
Yu, Xiaoqian and Kuckling, Dirk}, year={2019} }'
chicago: 'Herberg, Artjom, Xiaoqian Yu, and Dirk Kuckling. “End Group Stability
of Atom Transfer Radical Polymerization (ATRP)-Synthesized Poly(N-Isopropylacrylamide):
Perspectives for Diblock Copolymer Synthesis.” Polymers 11, no. 4 (2019).
https://doi.org/10.3390/polym11040678.'
ieee: 'A. Herberg, X. Yu, and D. Kuckling, “End Group Stability of Atom Transfer
Radical Polymerization (ATRP)-Synthesized Poly(N-isopropylacrylamide): Perspectives
for Diblock Copolymer Synthesis,” Polymers, vol. 11, no. 4, Art. no. 678,
2019, doi: https://doi.org/10.3390/polym11040678.'
mla: 'Herberg, Artjom, et al. “End Group Stability of Atom Transfer Radical Polymerization
(ATRP)-Synthesized Poly(N-Isopropylacrylamide): Perspectives for Diblock Copolymer
Synthesis.” Polymers, vol. 11, no. 4, 678, MDPI, 2019, doi:https://doi.org/10.3390/polym11040678.'
short: A. Herberg, X. Yu, D. Kuckling, Polymers 11 (2019).
date_created: 2022-04-21T09:08:41Z
date_updated: 2022-04-21T09:09:00Z
department:
- _id: '311'
doi: https://doi.org/10.3390/polym11040678
intvolume: ' 11'
issue: '4'
keyword:
- controlled radical polymerization
- atom transfer radical polymerization
- end group determination
- N-isopropylacrylamide
- block copolymerization
- smart polymers
- temperature sensitive polymers
- lower critical solution temperature
- ESI-TOF mass spectrometry
- ion mobility separation
- size exclusion chromatography
language:
- iso: eng
publication: Polymers
publication_status: published
publisher: MDPI
status: public
title: 'End Group Stability of Atom Transfer Radical Polymerization (ATRP)-Synthesized
Poly(N-isopropylacrylamide): Perspectives for Diblock Copolymer Synthesis'
type: journal_article
user_id: '94'
volume: 11
year: '2019'
...