{"article_number":"141","intvolume":" 10","citation":{"chicago":"Bürger, Julius, Vinay Kunnathully, Daniel Kool, Jörg Lindner, and Katharina Brassat. “Characterisation of the PS-PMMA Interfaces in Microphase Separated Block Copolymer Thin Films by Analytical (S)TEM.” Nanomaterials 10, no. 1 (2020). https://doi.org/10.3390/nano10010141.","mla":"Bürger, Julius, et al. “Characterisation of the PS-PMMA Interfaces in Microphase Separated Block Copolymer Thin Films by Analytical (S)TEM.” Nanomaterials, vol. 10, no. 1, 141, MDPI AG, 2020, doi:10.3390/nano10010141.","apa":"Bürger, J., Kunnathully, V., Kool, D., Lindner, J., & Brassat, K. (2020). Characterisation of the PS-PMMA Interfaces in Microphase Separated Block Copolymer Thin Films by Analytical (S)TEM. Nanomaterials, 10(1), Article 141. https://doi.org/10.3390/nano10010141","short":"J. Bürger, V. Kunnathully, D. Kool, J. Lindner, K. Brassat, Nanomaterials 10 (2020).","ieee":"J. Bürger, V. Kunnathully, D. Kool, J. Lindner, and K. Brassat, “Characterisation of the PS-PMMA Interfaces in Microphase Separated Block Copolymer Thin Films by Analytical (S)TEM,” Nanomaterials, vol. 10, no. 1, Art. no. 141, 2020, doi: 10.3390/nano10010141.","ama":"Bürger J, Kunnathully V, Kool D, Lindner J, Brassat K. Characterisation of the PS-PMMA Interfaces in Microphase Separated Block Copolymer Thin Films by Analytical (S)TEM. Nanomaterials. 2020;10(1). doi:10.3390/nano10010141","bibtex":"@article{Bürger_Kunnathully_Kool_Lindner_Brassat_2020, title={Characterisation of the PS-PMMA Interfaces in Microphase Separated Block Copolymer Thin Films by Analytical (S)TEM}, volume={10}, DOI={10.3390/nano10010141}, number={1141}, journal={Nanomaterials}, publisher={MDPI AG}, author={Bürger, Julius and Kunnathully, Vinay and Kool, Daniel and Lindner, Jörg and Brassat, Katharina}, year={2020} }"},"year":"2020","department":[{"_id":"15"},{"_id":"230"}],"author":[{"id":"46952","last_name":"Bürger","full_name":"Bürger, Julius","first_name":"Julius"},{"first_name":"Vinay","last_name":"Kunnathully","full_name":"Kunnathully, Vinay"},{"id":"44586","last_name":"Kool","full_name":"Kool, Daniel","first_name":"Daniel"},{"id":"20797","last_name":"Lindner","full_name":"Lindner, Jörg","first_name":"Jörg"},{"first_name":"Katharina","last_name":"Brassat","full_name":"Brassat, Katharina","id":"11305"}],"issue":"1","publisher":"MDPI AG","date_created":"2022-11-15T14:20:33Z","date_updated":"2023-01-10T12:11:57Z","_id":"34092","abstract":[{"text":"Block copolymer (BCP) self-assembly is a promising tool for next generation lithography as microphase separated polymer domains in thin films can act as templates for surface nanopatterning with sub-20 nm features. The replicated patterns can, however, only be as precise as their templates. Thus, the investigation of the morphology of polymer domains is of great importance. Commonly used analytical techniques (neutron scattering, scanning force microscopy) either lack spatial information or nanoscale resolution. Using advanced analytical (scanning) transmission electron microscopy ((S)TEM), we provide real space information on polymer domain morphology and interfaces between polystyrene (PS) and polymethylmethacrylate (PMMA) in cylinder- and lamellae-forming BCPs at highest resolution. This allows us to correlate the internal structure of polymer domains with line edge roughnesses, interface widths and domain sizes. STEM is employed for high-resolution imaging, electron energy loss spectroscopy and energy filtered TEM (EFTEM) spectroscopic imaging for material identification and EFTEM thickness mapping for visualisation of material densities at defects. The volume fraction of non-phase separated polymer species can be analysed by EFTEM. These methods give new insights into the morphology of polymer domains the exact knowledge of which will allow to improve pattern quality for nanolithography.","lang":"eng"}],"publication_identifier":{"issn":["2079-4991"]},"doi":"10.3390/nano10010141","publication":"Nanomaterials","title":"Characterisation of the PS-PMMA Interfaces in Microphase Separated Block Copolymer Thin Films by Analytical (S)TEM","keyword":["General Materials Science","General Chemical Engineering"],"status":"public","user_id":"77496","type":"journal_article","volume":10,"language":[{"iso":"eng"}],"publication_status":"published"}