Efficient Referencing of FSLG CPMAS HETCOR Spectra Using 2D 1H–1H MAS FSLG
B. Kumari, M. Brodrecht, T. Gutmann, H. Breitzke, G. Buntkowsky, Applied Magnetic Resonance 50 (2019) 1399–1407.
Download
No fulltext has been uploaded.
Journal Article
| English
Author
Kumari, Bharti;
Brodrecht, Martin;
Gutmann, TorstenLibreCat;
Breitzke, Hergen;
Buntkowsky, Gerd
Abstract
FSLG CPMAS HETCOR is a 2D solid-state NMR experiment which provides structural information and conformational correlation between a 1H and an X-nucleus. However, practical application of the experiment suffers from the chemical shift referencing problem on the indirect 1H dimension. In our paper, we present a novel 1H–1H MAS FSLG-based approach and its application to reference the FSLG CPMAS HETCOR which overcomes the 1H referencing in the 2D 1H-X HETCOR experiment. This approach works excellently irrespective of the sample type over a wide range of temperature.
Publishing Year
Journal Title
Applied Magnetic Resonance
Volume
50
Issue
12
Page
1399–1407
ISSN
LibreCat-ID
Cite this
Kumari B, Brodrecht M, Gutmann T, Breitzke H, Buntkowsky G. Efficient Referencing of FSLG CPMAS HETCOR Spectra Using 2D 1H–1H MAS FSLG. Applied Magnetic Resonance. 2019;50(12):1399–1407. doi:10.1007/s00723-019-01156-2
Kumari, B., Brodrecht, M., Gutmann, T., Breitzke, H., & Buntkowsky, G. (2019). Efficient Referencing of FSLG CPMAS HETCOR Spectra Using 2D 1H–1H MAS FSLG. Applied Magnetic Resonance, 50(12), 1399–1407. https://doi.org/10.1007/s00723-019-01156-2
@article{Kumari_Brodrecht_Gutmann_Breitzke_Buntkowsky_2019, title={Efficient Referencing of FSLG CPMAS HETCOR Spectra Using 2D 1H–1H MAS FSLG}, volume={50}, DOI={10.1007/s00723-019-01156-2}, number={12}, journal={Applied Magnetic Resonance}, author={Kumari, Bharti and Brodrecht, Martin and Gutmann, Torsten and Breitzke, Hergen and Buntkowsky, Gerd}, year={2019}, pages={1399–1407} }
Kumari, Bharti, Martin Brodrecht, Torsten Gutmann, Hergen Breitzke, and Gerd Buntkowsky. “Efficient Referencing of FSLG CPMAS HETCOR Spectra Using 2D 1H–1H MAS FSLG.” Applied Magnetic Resonance 50, no. 12 (2019): 1399–1407. https://doi.org/10.1007/s00723-019-01156-2.
B. Kumari, M. Brodrecht, T. Gutmann, H. Breitzke, and G. Buntkowsky, “Efficient Referencing of FSLG CPMAS HETCOR Spectra Using 2D 1H–1H MAS FSLG,” Applied Magnetic Resonance, vol. 50, no. 12, pp. 1399–1407, 2019, doi: 10.1007/s00723-019-01156-2.
Kumari, Bharti, et al. “Efficient Referencing of FSLG CPMAS HETCOR Spectra Using 2D 1H–1H MAS FSLG.” Applied Magnetic Resonance, vol. 50, no. 12, 2019, pp. 1399–1407, doi:10.1007/s00723-019-01156-2.
Google Scholar