Fructose as a Precursor for Mesoporous Carbon: Straightforward Solvent-Free Synthesis by Nanocasting

C. Weinberger, S. Haffer, T. Wagner, M. Tiemann, in: ACS Symposium Series, Washington, DC, 2014.

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Abstract
Due to their unique properties, ordered mesoporous carbon (OMC) materials prepared by nanocasting have raised great attention in recent years. Their synthesis usually comprises multiple cycles of impregnating a porous structure matrix with an aqueous solution of a suitable precursor, such as sucrose or other, often hazardous, compound. We present a more straightforward variation of this method by using fructose as the precursor compound. By using a solvent-free melt of the precursor, the impregnation requires only a single step. After carbonization by thermal decomposition and removal of the mesoporous silica structure matrix (SBA-15), ordered mesoporous carbon with one (CMK-3) or two (CMK-5) pore modes in two-dimensional, hexagonal symmetry (p6mm) is obtained.
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Weinberger C, Haffer S, Wagner T, Tiemann M. Fructose as a Precursor for Mesoporous Carbon: Straightforward Solvent-Free Synthesis by Nanocasting. In: ACS Symposium Series. ; 2014. doi:10.1021/bk-2014-1183.ch001
Weinberger, C., Haffer, S., Wagner, T., & Tiemann, M. (2014). Fructose as a Precursor for Mesoporous Carbon: Straightforward Solvent-Free Synthesis by Nanocasting. In ACS Symposium Series. https://doi.org/10.1021/bk-2014-1183.ch001
@inbook{Weinberger_Haffer_Wagner_Tiemann_2014, place={Washington, DC}, title={Fructose as a Precursor for Mesoporous Carbon: Straightforward Solvent-Free Synthesis by Nanocasting}, DOI={10.1021/bk-2014-1183.ch001}, booktitle={ACS Symposium Series}, author={Weinberger, Christian and Haffer, S. and Wagner, T. and Tiemann, Michael}, year={2014} }
Weinberger, Christian, S. Haffer, T. Wagner, and Michael Tiemann. “Fructose as a Precursor for Mesoporous Carbon: Straightforward Solvent-Free Synthesis by Nanocasting.” In ACS Symposium Series. Washington, DC, 2014. https://doi.org/10.1021/bk-2014-1183.ch001.
C. Weinberger, S. Haffer, T. Wagner, and M. Tiemann, “Fructose as a Precursor for Mesoporous Carbon: Straightforward Solvent-Free Synthesis by Nanocasting,” in ACS Symposium Series, Washington, DC, 2014.
Weinberger, Christian, et al. “Fructose as a Precursor for Mesoporous Carbon: Straightforward Solvent-Free Synthesis by Nanocasting.” ACS Symposium Series, 2014, doi:10.1021/bk-2014-1183.ch001.

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