Low Cycle Fatigue Performance of Additively Processed and Heat-Treated Ti-6Al-7Nb Alloy for Biomedical Applications

M. Hein, D. Kokalj, N.F. Lopes Dias, D. Stangier, H. Oltmanns, S. Pramanik, M. Kietzmann, K.-P. Hoyer, J. Meißner, W. Tillmann, M. Schaper, Metals 12 (2022).

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Hein, MaxwellLibreCat ; Kokalj, David; Lopes Dias, Nelson Filipe; Stangier, Dominic; Oltmanns, Hilke; Pramanik, Sudipta; Kietzmann, Manfred; Hoyer, Kay-PeterLibreCat; Meißner, Jessica; Tillmann, Wolfgang; Schaper, MirkoLibreCat
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Abstract
In biomedical engineering, laser powder bed fusion is an advanced manufacturing technology, which enables, for example, the production of patient-customized implants with complex geometries. Ti-6Al-7Nb shows promising improvements, especially regarding biocompatibility, compared with other titanium alloys. The biocompatible features are investigated employing cytocompatibility and antibacterial examinations on Al2O3-blasted and untreated surfaces. The mechanical properties of additively manufactured Ti-6Al-7Nb are evaluated in as-built and heat-treated conditions. Recrystallization annealing (925 °C for 4 h), β annealing (1050 °C for 2 h), as well as stress relieving (600 °C for 4 h) are applied. For microstructural investigation, scanning and transmission electron microscopy are performed. The different microstructures and the mechanical properties are compared. Mechanical behavior is determined based on quasi-static tensile tests and strain-controlled low cycle fatigue tests with total strain amplitudes εA of 0.35%, 0.5%, and 0.8%. The as-built and stress-relieved conditions meet the mechanical demands for the tensile properties of the international standard ISO 5832-11. Based on the Coffin–Manson–Basquin relation, fatigue strength and ductility coefficients, as well as exponents, are determined to examine fatigue life for the different conditions. The stress-relieved condition exhibits, overall, the best properties regarding monotonic tensile and cyclic fatigue behavior.</jats:p>
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Journal Title
Metals
Volume
12
Issue
1
Article Number
122
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Hein M, Kokalj D, Lopes Dias NF, et al. Low Cycle Fatigue Performance of Additively Processed and Heat-Treated Ti-6Al-7Nb Alloy for Biomedical Applications. Metals. 2022;12(1). doi:10.3390/met12010122
Hein, M., Kokalj, D., Lopes Dias, N. F., Stangier, D., Oltmanns, H., Pramanik, S., Kietzmann, M., Hoyer, K.-P., Meißner, J., Tillmann, W., & Schaper, M. (2022). Low Cycle Fatigue Performance of Additively Processed and Heat-Treated Ti-6Al-7Nb Alloy for Biomedical Applications. Metals, 12(1), Article 122. https://doi.org/10.3390/met12010122
@article{Hein_Kokalj_Lopes Dias_Stangier_Oltmanns_Pramanik_Kietzmann_Hoyer_Meißner_Tillmann_et al._2022, title={Low Cycle Fatigue Performance of Additively Processed and Heat-Treated Ti-6Al-7Nb Alloy for Biomedical Applications}, volume={12}, DOI={10.3390/met12010122}, number={1122}, journal={Metals}, publisher={MDPI AG}, author={Hein, Maxwell and Kokalj, David and Lopes Dias, Nelson Filipe and Stangier, Dominic and Oltmanns, Hilke and Pramanik, Sudipta and Kietzmann, Manfred and Hoyer, Kay-Peter and Meißner, Jessica and Tillmann, Wolfgang and et al.}, year={2022} }
Hein, Maxwell, David Kokalj, Nelson Filipe Lopes Dias, Dominic Stangier, Hilke Oltmanns, Sudipta Pramanik, Manfred Kietzmann, et al. “Low Cycle Fatigue Performance of Additively Processed and Heat-Treated Ti-6Al-7Nb Alloy for Biomedical Applications.” Metals 12, no. 1 (2022). https://doi.org/10.3390/met12010122.
M. Hein et al., “Low Cycle Fatigue Performance of Additively Processed and Heat-Treated Ti-6Al-7Nb Alloy for Biomedical Applications,” Metals, vol. 12, no. 1, Art. no. 122, 2022, doi: 10.3390/met12010122.
Hein, Maxwell, et al. “Low Cycle Fatigue Performance of Additively Processed and Heat-Treated Ti-6Al-7Nb Alloy for Biomedical Applications.” Metals, vol. 12, no. 1, 122, MDPI AG, 2022, doi:10.3390/met12010122.
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